Search results for "Ull"

From Laboratory Mixes Evaluation to Full Scale Test: Fatigue Behavior of Bio-Materials Recycled Asphalt Mixtures

2020

The present paper describes the full-scale accelerated test, carried out on asphalt pavements made up with bio-materials, especially designed to help reusing Reclaimed Asphalt (RA) by re-activating the aged binder. Four pavement sections were evaluated: three pavement sections with innovative bio-materials (bio-recycled asphalt mixtures), and a reference section with a conventional, high modulus asphalt mix (EME2). In this study, fatigue resistance was first evaluated in laboratory, with two-points bending test, and then at full scale under heavy traffic loading, with the IFSTTAR accelerated pavement testing facility. The evolution of bio-materials recycled asphalt mixture characteristics, …

Transition-Edge Sensors for Particle Induced X-ray Emission Measurements

2013

In this paper we present a new measurement setup, where a transitionedge sensor detector array is used to detect X-rays in particle induced X-ray emission measurements with a 2 MeV proton beam. Transition-edge sensors offer orders of magnitude improvement in energy resolution compared to conventional silicon or germanium detectors, making it possible to recognize spectral lines in materials analysis that have previously been impossible to resolve, and to get chemical information from the elements. Our sensors are cooled to the operation temperature (65 mK) with a cryogen-free adiabatic demagnetization refrigerator, which houses a specially designed X-ray snout that has a vacuum tight window…

Acetogenins from Annonaceae: Recent Progress in Isolation, Synthesis and Mechanisms of Action

2005

Covering: the literature from 1998 to 2004 The aim of the present review is to summarise the knowledge about newly isolated acetogenins (ACGs) in the last six years. It will also report the total syntheses that have allowed either the confirmation or the revision of some structures, together with the biological activities and mechanism of action of such interesting natural products. In fact, of the 417 isolated compounds reviewed, over 176 have been added during the period from 1998 to 2004.

Mechanism of crystallization of fast fired mullite-based glass–ceramic glazes for floor-tiles

2006

Abstract The mechanism of crystallization from a B 2 O 3 -containing glass, with composition based in the CaO–MgO–Al 2 O 3 –SiO 2 system, to a glass–ceramic glaze was studied by different techniques. Glass powder pellets were fast heated, simulating current industrial tile processing methods, at several temperatures from 700 to 1200 °C with a 5 min hold. Microstructural study by field emission scanning electron microscopy revealed that a phase separation phenomenon occurred in the glass, which promoted the onset of mullite crystallization at 900 °C. The amount of mullite in the glass heated between 1100 and 1200 °C was around 20 wt%, as determined by Rietveld refinement. The microstructure …

Effect of boron oxide on the microstructure of mullite-based glass-ceramic glazes for floor-tiles in the CaO–MgO–Al2O3–SiO2 system

2006

Abstract The effect of increasing replacement of Al2O3 by B2O3 in a parent glass on the sintering and further crystallization of mullite was investigated. The composition of the parent glass was chosen in the mullite primary phase field of the CaO–MgO–Al2O3–SiO2 quaternary system. Glass powder pellets were heated under standard (10 °C/min and 2 h of hold time) and fast heatings (25 °C/min and 5 min of hold time) at different temperatures from 700 to 1190 °C. Sintering of B2O3-containing glasses took place in the range between 850 and 1050 °C. X-ray diffraction results showed that mullite formed as unique crystalline phase for glasses containing amounts of B2O3 larger than 6 wt%. For lower a…

Role of Adrenomedullin in LSP-mediated lung injury

2014

An efficient esterification of pullulan using carboxylic acid anhydrides activated with iodine

2010

Received August 9, 2009Accepted January 12, 2010Published online February 11, 2010Acylation of alcohols (esterification) with anhydride is an important and routinely utilizedtransformation in organic synthesis. Iodine is a cheap and one of the most powerful anhy-dride activating agents for the esterification of alcohols. Therefore, an efficient and cost ef-fective method was developed for the acylation of pullulan polysaccharide by using differentacid anhydrides activated with iodine. A series of organo-soluble pullulan esters were suc-cessfully synthesized, purified and characterized. Under solvent free conditions, it was feasi-ble to fabricate pullulan nonaacetate and pullulan stearate. A…

El «Llibre de les Bèsties» (1287-1289) de Ramon Llull: anàlisi d'adaptacions infantils i juvenils

2020

En aquest article presentem una anàlisi de les sis adaptacions que del Llibre de les Bèsties (1287- 1289) es van publicar per al públic infantil i juvenil amb motiu de l’Any Llull (2015-2016). Després de presentar la figura de Ramon Llull com a escriptor de referència en l’època medieval i de situar Llibre de les Bèsties dins de la producció literària de Llull, analitzem els paratextos extratextuals i textuals de les sis adaptacions aquí estudiades. La presentació i l’anàlisi d’aquests paratextos ens permet determinar, d’una banda, a quin tipus de nivell lector va adreçada cada adaptació i quin treball didàctic en pot resultar; i, d’altra banda, com el missatge que Llull transmet en aquesta…

Endoscopic therapy of adenomas of the papilla of Vater. A retrospective analysis with long-term follow-up.

2001

Abstract Aims. To compare the efficacy and the complication rate between endoscopic snare resection of adenomas of Vater's papilla and endoscopic palliation. Methods. In a retrospective, non randomized manner, we compared long-term results of our endoscopic strategies in 36 patients with histologically confirmed adenoma of Vater's papilla submitted either to local endoscopic snare resection (n=18) or to simple endoscopic palliation (n=18), respectively. Results. Between 1985 and 1998 results were reviewed. Median age was 76.5 (range 42–89) years in the palliation, and 64.0(23–89) years in the endoscopic snare resection group. Median duration of follow-up was 33 (6–135) and 75.0 (27–123) mon…

Binostril versus mononostril approaches in endoscopic transsphenoidal pituitary surgery: clinical evaluation and cadaver study.

2016

OBJECTIVE Over the past 2 decades, endoscopy has become an integral part of the surgical repertoire for skull base procedures. The present clinical evaluation and cadaver study compare binostril and mononostril endoscopic transnasal approaches and the surgical techniques involved. METHODS Forty patients with pituitary adenomas were treated with either binostril or mononostril endoscopic surgery. Neurosurgical, endocrinological, ophthalmological, and neuroradiological examinations were performed. Ten cadaver specimens were prepared, and surgical aspects of the preparation and neuroradiological examination were documented. RESULTS In the clinical evaluation, 0° optics were optimal in the nas…