Search results for "complex analysis"
showing 10 items of 245 documents
Zero-Dimensional Hybrid Organic−Inorganic Lead Halides and Their Post-Synthesis Reversible Transformation into Three-Dimensional Perovskites
2021
Zero-dimensional (0D) mixed-halide hybrid organic-inorganic MA4PbX6·2H2O (MA = CH3NH3+; X = Br1 - xIx with 0 < x < 1) has been synthesized by a solvent-free mechanochemical approach. It has been shown that this 0D phase with sharp absorption features in the near-UV is a hydrated structure, which can be reversibly transformed into the three-dimensional perovskite phase MAPbX3 by simple thermal annealing (dehydration) in air. This work reveals a new approach to hybrid organic-inorganic perovskites and related 0D structures, which have so far only been thoroughly studied for the inorganic Cs4PbX6 compounds. Hetero-structures for Efficient Luminescent Devices (HELD) REFERENCIA: 834431 PCIN-2019…
Determination at low ppm levels of dithiocarbamate residues in foodstuff by vapour phase-liquid phase microextraction-infrared spectroscopy
2010
Abstract A methodology based on the vapour phase (VP) generation of carbon disulphide from non-volatile dithiocarbamate compounds has been developed for determination of pesticide residues in foodstuff at low ppm levels. The method involves a selective reaction combined with liquid phase microextraction (LPME) and transmission infrared measurements. The use of a home made transmission cell improved the detection limits (LOD) compared to the use of attenuated total reflectance measurements by a factor of approximately 80. Using the most appropriate experimental conditions for the CS2 generation and LPME preconcentration, the precision of the methodology, expressed as the relative standard de…
Second zero dispersion wavelength measurement through soliton self-frequency shift compensation in suspended core fibre
2008
International audience; A simple experimental technique to evaluate the second zero dispersion wavelength of very small core microstrutured fibres is described. Based on the effect of soliton self-frequency shift and its subsequent compensation in the vicinity of the second zero dispersion. the proposed method is applied to both standard and suspended core microstructured fibres by simply measuring the frequency stabilised soliton spectrum, avoiding any calculation and knowledge of any experimental parameters.
Learning complex analysis in different branches – Project Spotlight-Y for future teachers
2018
International audience; At the University of Bremen in teaching complex analysis, we split the last part of the lecture into two branches according to profession: While future mathematicians deepen their understanding in a branch for them, future teachers take a branch of the lecture where they prepare a task with dynamical geometry software for pupils which is based on phenomena of complex analysis. Here, we describe the design of the course, some general aims and first results obtained from the branch for future teachers.
Classification of vegetable oils according to their botanical origin using amino acid profiles established by High Performance Liquid Chromatography …
2010
Abstract A preliminary study using amino acid profiles to classify oils according to their botanical origin has been performed. Amino acid profiles were obtained from hydrolysis of proteins present in vegetable oils, and established by High Performance Liquid Chromatography (HPLC) with UV–vis detection. Proteins present in hazelnut, corn, soybean, olive, avocado, peanut and grapeseed oils were precipitated with acetone, and the residue was hydrolysed in acid medium. The amino acids obtained were derivatized with o -phthaldialdehyde and separated by HPLC. Peaks corresponding to 18 amino acids were observed using a C18 column and a gradient of acetonitrile–water in the presence of a 5 mM citr…
Comparative Analyses between the Zero-Inertia and Fully Dynamic Models of the Shallow Water Equations for Unsteady Overland Flow Propagation
2018
The shallow water equations are a mathematical tool widely applied for the simulation of flow routing in rivers and floodplains, as well as for flood inundation mapping. The interest of many researchers has been focused on the study of simplified forms of the original set of equations. One of the most commonly applied simplifications consists of neglecting the inertial terms. The effects of such a choice on the outputs of the simulations of flooding events are controversial and are an important topic of debate. In the present paper, two numerical models recently proposed for the solution of the complete and zero-inertia forms of the shallow water equations, are applied to several unsteady f…
Rationally designed haptens for highly sensitive monoclonal antibody-based immunoanalysis of fenhexamid.
2018
Immunochemical methods have been consolidated during the last few years as complementary analytical strategies for chemical contaminant and residue determination. However, generation of suitable immunoreagents for small organic molecules demands adequate hapten design. In this study, fenhexamid was considered as a model compound and novel haptens were designed and synthesized in order to evaluate the influence of the linker tethering site on antibody binding properties and immunoassay parameters. Haptens were conceived with the spacer arm at different positions, while the more antigenic aromatic moiety was kept free. The synthesis of these functionalized compounds was accomplished by total …
Numerical construction of the density-potential mapping
2018
We demonstrate how a recently developed method Nielsen et al. [Nielsen et al., EPL 101, 33001 (2013)] allows for a comprehensive investigation of time-dependent density functionals in general, and of the exact time-dependent exchange-correlation potential in particular, by presenting the first exact results for two- and three-dimensional multi-electron systems. This method is an explicit realization of the Runge–Gross correspondence, which maps time-dependent densities to their respective potentials, and allows for the exact construction of desired density functionals. We present in detail the numerical requirements that makes this method efficient, stable and precise even for large and rap…
Zero-Achievers Non-Progressing Studies in Finnish Open University : Three Preventive Factors
2021
Current education policy responds to changes and needs in working life by guiding individuals at different stages of working careers to develop their skills in the spirit of lifelong learning. More and more are applying with hope and enthusiasm to the Open University to strengthen their competence but are unable to get their studies completed. The article explores factors related to the non-progression of studies by students at the Open University in Finland. We call non-progressing students zero-achievers who enroll in studies but do not complete a single credit during the period of course. This research is a descriptive mixed methods study. The research data was collected by an online sur…
Net currents obtained from zero-average potentials in single amphoteric nanopores
2013
We have studied experimentally and theoretically the rectifying properties of a single asymmetric nanopore functionalized with amphoteric lysine groups and characterized the net current obtained with zero-average time dependent potentials. The pH-controlled rectification phenomena may be relevant to bio-electrochemistry, pH sensing and regulation, and energy conversion. (C) 2013 Elsevier B.V. All rights reserved.