Search results for "complex"

showing 10 items of 5889 documents

Azide Binding Controlled by Steric Interactions in Second Sphere. Synthesis, Crystal Structure, and Magnetic Properties of [Ni II 2 (L)(μ 1,1 -N 3 )]…

2016

International audience; The dinuclear Ni-II complex [Ni-2(L-2)][ClO4](2) (3) supported by the 28-membered hexaaza-dithiophenolate macro-cycle (L-2)(2-) binds the N-3(-) ion specifically end-on yielding [Ni-2(L-2)(mu(1,1)-N-3)] [ClO4] (7) or [Ni-2(L-2)(mu(1,1)-N-3)][BPh4] (8), while the previously reported complex [Ni2L1(mu(1,3)-N-3)][ClO4] (2) of the 24-membered macrocycle (L-1)(2-) coordinates it in the end-to-end fashion. A comparison of the X-ray structures of 2, 3, and 7 reveals the form-selective binding of complex 3 to be a consequence of its preorganized, channel-like binding pocket, which accommodates the azide anion via repulsive CH center dot center dot center dot pi interactions …

Steric effectsequilibrium-constantsStereochemistrytransition-metal-complexesCrystal structure010402 general chemistry01 natural sciences[ CHIM ] Chemical Sciencessolvation free-energyInorganic Chemistrychemistry.chemical_compoundtetranuclear nickel(ii) complexes[CHIM.CRIS]Chemical Sciences/CristallographyAntiferromagnetismMolecule[CHIM.COOR]Chemical Sciences/Coordination chemistryPhysical and Theoretical Chemistrymu-azidoEquilibrium constantmolecular-structure010405 organic chemistryChemistryLigandni-ii[ CHIM.INOR ] Chemical Sciences/Inorganic chemistryend-to-end0104 chemical sciencesexchange interactionsCrystallographyAzideGround stateorbital interactions[ CHIM.RADIO ] Chemical Sciences/Radiochemistry
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Exceedingly Fast Oxygen Atom Transfer to Olefins via a Catalytically Competent Nonheme Iron Species

2016

El mateix article està publicat en alemany a l'edició alemanya d' 'Angewandte Chemie' (ISSN 0044-8249, EISSN 1521-3757), 2016, vol. 128, núm. 21, p.6418–6422. DOI http://dx.doi.org/10.1002/ange.201601396 The reaction of [Fe(CF3SO3)2(PyNMe3)] with excess peracetic acid at −40 °C leads to the accumulation of a metastable compound that exists as a pair of electromeric species, [FeIII(OOAc)(PyNMe3)]2+ and [FeV(O)(OAc)(PyNMe3)]2+, in fast equilibrium. Stopped-flow UV/Vis analysis confirmed that oxygen atom transfer (OAT) from these electromeric species to olefinic substrates is exceedingly fast, forming epoxides with stereoretention. The impact of the electronic and steric properties of the subs…

Steric effectsoxidationIronKineticsAlkenes010402 general chemistryMedicinal chemistry01 natural sciencesCatalysisCatalysisReaction ratechemistry.chemical_compoundPeracetic acidMetastabilityepoxidationEpòxidsOrganic chemistryChemistry010405 organic chemistrySubstrate (chemistry)General Chemistrynonheme iron complexesGeneral MedicineEpoxy compoundsNonheme iron0104 chemical sciencesAlquenskineticsolefinsFerroAngewandte Chemie
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Panel Summary:Multistimuli and Different Sensory Modalities

1999

Our everyday environment in which we live is characterised by stimuli capable of eliciting our actions (or reactions). Generally our actions are influenced by a number of stimuli which are multimodal.

Stimulus modalitybacteriaSingle photon absorptionequipment and suppliesPsychologycomplex mixturesNeuroscience
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Einstein-Smoluchowsky equation handled by complex fractional moments

2014

In this paper the response of a non linear half oscillator driven by α-stable white noise in terms of probability density function (PDF) is investigated. The evolution of the PDF of such a system is ruled by the so called Einstein-Smoluchowsky equation involving, in the diffusive term, the Riesz fractional derivative. The solution is obtained by the use of complex fractional moments of the PDF, calculated with the aid of Mellin transform operator. It is shown that solution can be found for various values of stability index α and for any nonlinear function of the drift term in the stochastic differential equation.

Stochastic partial differential equationNonlinear systemStochastic differential equationMellin transformDifferential equationOperator (physics)Mathematical analysisProbability density functiona-stable white noise Nonlinear systems Einstein-Smoluchowsky equation Complex fractional momentsFractional calculusMathematics
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Physics of the nuclear pore complex: Theory, modeling and experiment

2021

Abstract The hallmark of eukaryotic cells is the nucleus that contains the genome, enclosed by a physical barrier known as the nuclear envelope (NE). On the one hand, this compartmentalization endows the eukaryotic cells with high regulatory complexity and flexibility. On the other hand, it poses a tremendous logistic and energetic problem of transporting millions of molecules per second across the nuclear envelope, to facilitate their biological function in all compartments of the cell. Therefore, eukaryotes have evolved a molecular “nanomachine” known as the Nuclear Pore Complex (NPC). Embedded in the nuclear envelope, NPCs control and regulate all the bi-directional transport between the…

Stochastic transportMolecular modelingGeneral Physics and AstronomyComputational biologyMolecular dynamics01 natural sciencesGenomeArticleDiffusionNanochannels0103 physical sciencesotorhinolaryngologic diseasesmedicineNuclear pore010306 general physicsPhysicsComputational modelIntrinsically disordered proteins010308 nuclear & particles physicsCompartmentalization (psychology)Nuclear pore complexCell nucleusCrowdingmedicine.anatomical_structureCytoplasmMultivalencyBiomimeticNucleusFunction (biology)Physics Reports
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A paradigm of extreme rainfall pluvial floods in complex urban areas: the flood event of 15 July 2020 in Palermo (Italy)

2021

Abstract. In the last few years, some regions of the Mediterranean area have witnessed a progressive increase in extreme events, such as urban and flash floods, as a response to the increasingly frequent and severe extreme rainfall events, which are often exacerbated by the ever-growing urbanization. In such a context, the urban drainage systems may not be sufficient to convey the rainwater, thus increasing the risk deriving from the occurrence of such events. This study focuses on a particularly intense urban flood that occurred in Palermo (Italy) on 15 July 2020; it represents a typical pluvial flood due to extreme rainfall on a complex urban area that many cities have experienced in rece…

StormwaterContext (language use)Urban areaEnvironmental technology. Sanitary engineeringUrban floodGbest management practicesHuman settlementUrbanizationGeography. Anthropology. RecreationFlash floodGE1-350TD1-1066natural based solutionsQE1-996.5geographygeography.geographical_feature_categoryFlood mythGeologycomplex urban areaEnvironmental sciencesextreme rainfallfloodabilityPluvialGeneral Earth and Planetary Sciencesfloods modelingWater resource managementNatural Hazards and Earth System Sciences
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(Strept)avidin as host for biotinylated coordination complexes: stability, chiral discrimination, and cooperativity

2005

Incorporation of a biotinylated ruthenium tris(bipyridine) [Ru(bpy)₂(Biot-bpy)]²⁺ (1) in either avidin or streptavidin-(strept)avidin-can be conveniently followed by circular dichroism spectroscopy. To determine the stepwise association constants, cooperativity, and chiral discrimination properties, diastereopure (Λ and δ)-1 species were synthesized and incorporated in tetrameric (strept)avidin to afford (δ-[Ru(bpy)₂(Biot-bpy)]²⁺)x⊂avidin, (Λ- [Ru(bpy)₂(Biot-bpy)]²⁺)x⊂avidin, (δ-[Ru(bpy)₂(Biot- bpy)]²⁺)x⊂streptavidin, and (Λ-[Ru(bpy)₂(Biot-bpy)]²⁺) x⊂streptavidin (x = 1-4) For these four systems, the overall stability constants are log β₄ = 28.6, 30.3, 36.2, and 36.4, respectively. Critical…

StreptavidinCircular dichroismProtein ConformationStereochemistryBiotinchemistry.chemical_elementCooperativity010402 general chemistry01 natural sciencesInorganic ChemistryStructure-Activity RelationshipBipyridinechemistry.chemical_compound22'-DipyridylBacterial ProteinsBiotinCoordination ComplexesBiotinylation[CHIM.COOR]Chemical Sciences/Coordination chemistryPhysical and Theoretical ChemistryComputingMilieux_MISCELLANEOUSMolecular Structurebiology010405 organic chemistry[ CHIM.COOR ] Chemical Sciences/Coordination chemistryAvidinProtein Structure Tertiary0104 chemical sciencesRuthenium[CHIM.THEO]Chemical Sciences/Theoretical and/or physical chemistryCrystallographychemistryBiotinylation[ CHIM.THEO ] Chemical Sciences/Theoretical and/or physical chemistrybiology.proteinStreptavidinAvidin
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String Attractors and Infinite Words

2022

The notion of string attractor has been introduced by Kempa and Prezza (STOC 2018) in the context of Data Compression and it represents a set of positions of a finite word in which all of its factors can be “attracted”. The smallest size γ∗ of a string attractor for a finite word is a lower bound for several repetitiveness measures associated with the most common compression schemes, including BWT-based and LZ-based compressors. The combinatorial properties of the measure γ∗ have been studied in [Mantaci et al., TCS 2021]. Very recently, a complexity measure, called string attractor profile function, has been introduced for infinite words, by evaluating γ∗ on each prefix. Such a measure has…

String attractorSettore INF/01 - InformaticaFactor complexityMorphismSturmian wordRecurrent wordRepetitiveness measure
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Metabolism and Lysine Biosynthesis Control in Brevibacterium Flavum: Impact of Stringent Response in Bacterial Cells

2005

Parameters affecting lysine biosynthesis by Brevibacterium flavum RC 115 cells under stringent response conditions (test guanosine 5′-diphosphate 3′-diphosphate accumulation in cells) caused by threonine limitation were investigated. Experimental results confirmed that an increase in lysine biosynthesis by this bacterium under stringent response conditions might be a result of an increase in the intracellular concentration of NADPH as well as lysine export activity.

Stringent responseLysineGuanosineMetabolismBiologycomplex mixturesCorynebacterium glutamicumchemistry.chemical_compoundchemistryBiochemistryBrevibacterium flavumbacteriaThreonineIntracellular
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Structure and function of human BMAL1–CLOCK–DNA complex

2011

Structural BiologyChemistryComputational biologyDna complexStructure and functionActa Crystallographica Section A Foundations of Crystallography
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