0000000000141518
AUTHOR
Farid Chemat
Solvent-free microwave-assisted extraction of polyphenols from olive tree leaves: Antioxidant and antimicrobial properties
International audience; Response surface methodology (RSM) and artificial neural networks (ANN) were evaluated and compared in order to decide which method was the most appropriate to predict and optimize total phenolic content (TPC) and oleuropein yields in olive tree leaf (Olea europaea) extracts, obtained after solvent-free microwave- assisted extraction (SFMAE). The SFMAE processing conditions were: microwave irradiation power 250-350 W, extraction time 2-3 min, and the amount of sample 5-10 g. Furthermore, the antioxidant and antimicrobial activities of the olive leaf extracts, obtained under optimal extraction conditions, were assessed by several in vitro assays. ANN had better predic…
Green food processing: concepts, strategies, and tools
Abstract One of the developmental aspects of food science is testing and adapting advanced technologies for food production, which save resources and improve food quality. More often than not, this includes technologies operating at lower temperatures, shorter time, and resulting in better preservation of the thermolabile compounds in the foods, as compared to conventional technologies. Nutritionally rich but thermally sensitive raw materials such as fruit, vegetables, meats, and others can particularly benefit from the application of such advanced food technologies. Technologies with the most tested potential for industrial implementation include nonthermal plasma, pulsed electric field, h…
A review of sustainable and intensified techniques for extraction of food and natural products
International audience; This review presents innovative extraction techniques and their role in promoting sustainable ingredients forthe food, cosmetic and pharmaceutical industries. These techniques (such as microwave, ultrasound, pulseelectricfield, instant controlled pressure drop, sub- and super-criticalfluid processing, extrusion, mechano-chemistry, high pressure, and ohmic, UV and IR heating) use or produce less solvent, energy, and hazards.This review will provide the necessary theoretical background and some details about green extractiontechniques, their mechanisms, some applications, and environmental impacts. We will pay special attentionto the strategies and present them as succ…
Editorial overview: Green analytical chemistry
International audience
Determination of fatty acids and lipid classes in salmon oil by near infrared spectroscopy
International audience; Near-infrared (NIR) spectroscopy was evaluated as a rapid method for the determination of oleic, palmitic, linoleic and linolenic acids as well as omega-3, omega-6, and to predict polyunsaturated, monounsaturated and saturated fatty acids, together with triacylglycerides, diglycerides, free fatty acids and ergosterol in salmon oil. To do it, Partial Least Squares (PLS) regression models were applied to correlate NIR spectra with aforementioned fatty acids and lipid classes. Results obtained were validated in front of reference procedures based on high performance thin layer and gas chromatography. PLS-NIR has a good predictive capability with relative root mean squar…
Citrus aurantium L. Active Constituents, Biological Effects and Extraction Methods. An Updated Review
Citrus genus is a prominent staple crop globally. Long-term breeding and much hybridization engendered a myriad of species, each characterized by a specific metabolism generating different secondary metabolites. Citrus aurantium L., commonly recognized as sour or bitter orange, can exceptionally be distinguished from other Citrus species by unique characteristics. It is a fruit with distinctive flavor, rich in nutrients and phytochemicals which possess different health benefits. This paper presents an overview of the most recent studies done on the matter. It intends to provide an in-depth understanding of the biological activities and medicinal uses of active constituents existing in C. au…
Portability in analytical chemistry: a green and democratic way for sustainability
International audience; Recent advances in portability of analytical equipment have been considered to enlighten the advantages offered by portable instrumentation on greening the analytical methods. Their use drastically reduces sampling, sample stockage, and transport, thus avoiding environmental side effects and risks, also improving decision-making. The fact that portable instrumentation is, in general, less expensive than bench instruments and apparatuses makes also available the analytical tools for extended sectors of the population, thus making accessible the advantages derived from analytical methods. The role of sensor technology and portable miniaturized systems has been consider…
Extraction Methods of Essential Oils From Herbs and Spices
International audience; This chapter describes both conventional and non‐conventional extraction methods of essential oils (EOs) from herbs and spices. Although hydrodistillation, steam distillation and solvent extraction are the most applied methods, several non‐conventional technologies have been evaluated, especially in respect to EO recovery, and a great potential has been attributed to these non‐conventional methods. For instance, ultrasound, microwave, supercritical fluid, pulsed electric fields, ohmic‐heating and microwave (MW) extraction techniques applied alone or combined with other techniques are potent tools to obtain EOs in a 'green' way from natural resources such as aromatic …
High Yields of Shrimp Oil Rich in Omega-3 and Natural Astaxanthin from Shrimp Waste
A valued marine oil rich in omega-3 lipids and natural astaxanthin is obtained with remarkably high yield (up to S wt %) extending to pink shrimp waste (head and carapace) using the approach to extract fish oil from fish processing byproducts using D-limonene. Biobased limonene is an excellent solvent for both unsaturated lipids and astaxanthin-based carotenoids preventing oxidative degradation during the extraction cycle including solvent separation at 85 degrees C. Explaining the deep red color of the shrimp oil obtained, computational simulation suggests that D-limonene is also a good solvent for natural astaxanthin abundant in shrimp.
Omega-3 Extraction from Anchovy Fillet Leftovers with Limonene: Chemical, Economic, and Technical Aspects
International audience; We investigate selected chemical, technical, and economic aspects of the production of fish oil rich in polyunsaturated omega-3 fatty acids from anchovy filleting leftovers using d-limonene as the extraction solvent at ambient temperature and pressure. Entirely derived from the orange peel prior to orange squeezing for juice production, the bio-based solvent is easily recovered, affording a circular economy process with significant potential for practical applications.
Portable microwave assisted extraction: An original concept for green analytical chemistry.
International audience; This paper describes a portable microwave assisted extraction apparatus (PMAE) for extraction of bioac-tive compounds especially essential oils and aromas directly in a crop or in a forest. The developed procedure, based on the concept of green analytical chemistry, is appropriate to obtain direct in-field information about the level of essential oils in natural samples and to illustrate green chemical lesson and research. The efficiency of this experiment was validated for the extraction of essential oil of rosemary directly in a crop and allows obtaining a quantitative information on the content of essential oil, which was similar to that obtained by conventional m…
Solar radiation as a prospective energy source for green and economic processes in the food industry: From waste biomass valorization to dehydration, cooking, and baking
International audience; Solar energy has recently attracted the attention of both industry and academia, to be used as a source of clean energy for green production of various products such as food-related commodities. This review aims to explore the applicability of this green energy source for extraction of valuable components (e.g., bioactive compounds and essential oils) from plant materials and waste biomass, dehydration of plant materials, water recovery through desalination, decontamination, cooking, and baking of agri-food products. According to the literature, concentrated solar power systems (CSP) have been successfully employed for bioactive compounds (e.g. essential oils) extrac…
Thermodynamics, transport phenomena, and electrochemistry of external field-assisted nonthermal food technologies
Interest in the development and adoption of nonthermal technologies is burgeoning within the food and bioprocess industry, the associated research community, and among the consumers. This is evident from not only the success of some innovative nonthermal technologies at industrial scale, but also from the increasing number of publications dealing with these topics, a growing demand for foods processed by nonthermal technologies and use of natural ingredients. A notable feature of the nonthermal technologies such as cold plasma, electrohydrodynamic processing, pulsed electric fields, and ultrasound is the involvement of external fields, either electric or sound. Therefore, it merits to study…
Extraction of bioactive compounds and essential oils from mediterranean herbs by conventional and green innovative techniques: A review
International audience; Market interest in aromatic plants from the Mediterranean is continuously growing mainly due to their medicinal and bioactive compounds (BACs) with other valuable constituents from essential oils (EOs). From ancient times, these plants have been important condiments for traditional Mediterranean cuisine and remedies in folk medicine. Nowadays, they are considered as important factors for food quality and safety, due to prevention of various deteriorative factors like oxidations and microbial spoilage. EOs have different therapeutic benefits (e.g. antioxidant, anti-inflammatory, antimicrobial, and antifungal), while BACs mostly affect nutritive, chemical, microbiologi…