0000000000495409
AUTHOR
Frédéric Désévédavy
Visible Light Generation and its Influence on Supercontinuum in Chalcogenide As2S3 Microstructured Optical Fiber
We demonstrate visible light generation in chalcogenide As2S3 microstructured optical fiber. The generated visible light causes irreversible damage to the fiber core because of the high absorption coefficient of chalcogenide glasses in the visible band. The SCs (supercontinua) are measured in both untapered and tapered As2S3 fibers, no wider SC is obtained in the tapered one. The SC growth is prevented by the visible light generation since the damage to the fiber core decreases the fiber transmission substantially. This effect can be avoided by designing the fiber to enable the pump source to work in single-mode operation.
Microstructured Optical Fibers from As2S3 Glass for Fiber Optics Sources in the MIR range
International audience
Recent developments in chalcogenide photonic crystal fibres
Elaboration of low-losses highly non linear chalcogenide optical fibers for the generation of efficient non linear effects in the infrared remains a challenge. In recent years, much work has been devoted to the study of microstructured optical fibers (MOFs) with different designs and various elaboration processes. Their background losses were typically of several dB/m.
Impact of optical and structural aging in As_2S_3 microstructured optical fibers on mid-infrared supercontinuum generation
We analyze optical and structural aging in As2S3 microstructured optical fibers (MOFs) that may have an impact on mid-infrared supercontinuum generation. A strong alteration of optical transparency at the fundamental OH absorption peak is measured for high-purity As2S3 MOF stored in atmospheric conditions. The surface evolution and inherent deviation of corresponding chemical composition confirm that the optical and chemical properties of MOFs degrade upon exposure to ambient conditions because of counteractive surface process. This phenomenon substantially reduces the optical quality of the MOFs and therefore restrains the spectral expansion of generated supercontinuum. This aging process …
Synthesis and characterization of chalcogenide glasses from the system Ga-Ge-Sb-S and preparation of a single-mode fiber at 1.55 μm
International audience; The aim of this work is to study different compositions in the Ga-Ge-Sb-S system for the definition of two compositions compatible with the elaboration of a single-mode fiber at the 1.55 μm telecom wavelength. The variations of the glass transition temperature (Tg), the dilatation coefficient (α) and the refractive index (n) have been studied for two glasses series: GaxGe25−xSb10S65 (series 1), Ga5Ge25−xSb10S60+x (series 2). This study has lead to the choice of the Ga4Ge21Sb10S65 composition as clad glass for the preparation of the single-mode fiber and Ga5Ge20Sb10S65 composition as the core. The discrepancies for the studied parameters between the core and clad comp…
Chalcogenide Microstructured Fibers for Infrared Systems, Elaboration, Modelization, and Characterization
special issue " Fiber Optic Research in France " (Part III of III); International audience; Chalcogenide fibers present numerous possible applications in the IR field. For many applications, single mode fibers must be obtained. An original way is the realization of microstructured optical fibers (MOFs) with solid core. These fibers present a broad range of optical properties thanks to the high number of freedom degrees of their geometrical structure. In this context, we have developed MOFs for near and mid IR transmission with different geometries and properties such as multimode or endless single-mode operation, small or large mode area fibers. We have also investigated numerically the mai…
Octave-spanning coherent supercontinuum generation in a step-index tellurite fiber and towards few-cycle pulse compression at 2 μ m
Abstract We experimentally demonstrate 140-THz bandwidth (at −20 dB) supercontinuum generation in a 10 cm-long all-normal dispersion step-index tellurite fiber pumped by a turn-key femtosecond fiber laser emitting at 2 . 11 μ m at a repetition rate of 19 MHz. The soliton self-frequency shifted thulium-doped fiber mode-locked laser emits initial transform-limited pulses, with 85-fs pulse duration, that are subsequently quasi-linearly chirped (over more than 50 THz) during the above nJ-level nonlinear propagation. Moreover, we numerically demonstrate the possible pulse compression down to 12 fs by means of additional linear propagation in a standard step-index fluoride fiber with anomalous di…
Visible Light Generation and Its Influence to Supercontinuum in As2S3 Microstructured Fiber
We demonstrate visible light generation in As 2 S 3 microstructured fiber for the first time. It limits the spectral range of supercontinuum. The visible light generation can be avoided by designing the fiber for the single-mode operation.
Elaboration by casting method of low losses chalcogenide microstructured fibers for near and mid infrared applications
oral session C " Preparation and Property ", oral [TuA-16]; International audience
Recent developments in chalcogenide PCF
International audience
Small-core chalcogenide microstructured fibers for the infrared.
International audience; We report several small-core chalcogenide microstructured fibers fabricated by the "Stack & Draw" technique from Ge(15)Sb(20)S(65) glass with regular profiles. Mode field diameters and losses have been measured at 1.55 microm. For one of the presented fibers, the pitch is 2.5 microm, three times smaller than that already obtained in our previous work, and the corresponding mode field diameter is now as small as 3.5 microm. This fiber, obtained using a two step "Stack & Draw" technique, is single-mode at 1.55 microm from a practical point of view. We also report the first measurement of the attenuation between 1 and 3.5 microm of a chalcogenide microstructured fiber. …
TeO2-ZnO-La2O3 tellurite glass system investigation for mid-infrared robust optical fibers manufacturing
Abstract TeO2-ZnO-La2O3 (TZL) ternary glasses were investigated in order to manufacture step-index optical fibers with low optical losses in the near- and mid-infrared ranges and superior mechanical properties. To identify appropriate TZL glass compositions for optical fibers manufacturing, the whole vitreous domain of the ternary diagram was explored by characterizing bulk samples from thermal and optical point of view. Investigations were focused on understanding how the refractive index evolves as a function of the composition. For this, several parameters were analyzed such as density, molar volume, oxygen packing density, molar refractivity, polarizability and optical basicity. Finally…
Mid-infrared supercontinuum generation from 2 to 14 μm in various chalcogenide glasses optical fibers
Chalcogenide glasses optical fibers with step index or microstructured profiles are drawn from low toxicity compositions. Supercontinuum generation lead to an infrared spectrum spanning from 2 to 14µm with a 10µm core fiber of 40mm length.
3.5-μm bandwidth mid-infrared supercontinuum generation in a 2-cm long suspended-core chalcogenide fiber
A supercontinuum source extending from 0.6 to 4.1 µm has been successfully generated in a 2-cm long As2S3 chalcogenide suspended-core fiber by means of a nJ-level 200-fs pumping at 2.5 µm.
Atmospheric aging and surface degradation in As2S3 fibers in relation with suspended-core profile
Abstract Microstructured optical fibers (MOF) can be seen as next generation fiber of significance in advancing the compact optics because of its excellent compatibility in integrated optics. However, the degradation of their physicochemical properties limits their efficiency and lifetime. Atmospheric moisture is responsible for the degradation of amorphous systems especially chalcogenide glasses. In the light of previously reported studies, in order to clarify the aging process continuously evolving in sulfide microstructured optical fiber over time, a detailed investigation of this phenomenon has been conducted. The time-dependent transmission and glass chemical deterioration have been st…
Enhanced supercontinuum generation in tapered tellurite suspended core fiber
Abstract We demonstrate 400-THz (0.6–3.3 µm) bandwidth infrared supercontinuum generation in a 10 cm-long tapered tellurite suspended core fiber pumped by nJ-level 200-fs pulses from an optical parametric oscillator. The increased nonlinearity and dispersion engineering extended by the moderate reduction of the fiber core size are exploited for supercontinuum optimization on both frequency edges (i.e., 155-THz overall gain), while keeping efficient power coupling into the untapered fiber input. The remaining limitation of supercontinuum bandwidth is related to the presence of the high absorption beyond 3 µm whereas spectral broadening is expected to fully cover the glass transmission window…
Filament-induced visible-to-mid-IR supercontinuum in a ZnSe crystal: Towards multi-octave supercontinuum absorption spectroscopy
Abstract We report on the generation of multiple-octave supercontinuum laser source spanning from 0.5 μm to 11 μm induced by multi-filamentation in a ZnSe crystal. The generated supercontinuum is both spatially and spectrally characterized. It is then exploited in a proof-of-principle experiment for methane spectroscopy measurements by means of the supercontinuum absorption spectroscopy technique. The entire absorption spectrum is successfully recorded within the whole spectral bandwidth of the supercontinuum. Experimental results are in fairly good agreement with the HITRAN database, confirming the reliability and stability over several hours of the generated supercontinuum.
Chalcogenide glass hollow core photonic crystal fibers
International audience; We report the first hollow core photonic crystal fibers (HC PCF) in chalcogenide glass. To design the required HC PCF profiles for such high index glass, we use both band diagram analysis to define the required photonic bandgap and numerical simulations of finite size HC PCFs to compute the guiding losses. The material losses have also been taken into account to compute the overall losses of the HC PCF profiles. These fibers were fabricated by the stack and draw technique from Te20As30Se50 (TAS) glass. The fibers we drew in this work are composed of six rings of holes and regular microstructures. Two profiles are presented, one is known as a kagome lattice and the ot…
Mid-infrared supercontinuum generation in suspended-core Chalcogenide and Tellurite optical fibers
We report the experimental generation of mid-infrared supercontinuum in tellurite and chalcogenide suspended-core fibers pumped close to their zero-dispersion in femtosecond regime. The resulting supercontinua extend until 2.8µm in tellurite and 3.2µm in chalcogenide fibers.
Multioctave midinfrared supercontinuum generation in suspended-core chalcogenide fibers
An As2S3 fiber-based supercontinuum source that covers 3500 nm, extending from near visible to the midinfrared, is successfully reported by using a 200-fs-pulsed pump with nJ-level energy at 2.5 μm. The main features of our fiber-based source are two-fold. On the one hand, a low-loss As2S3 microstructured optical fiber has been fabricated, with typical attenuation below 2 dB/m in the 1-4 μm wavelength range. On the other hand, a 20-mm-long microstructured fiber sample is sufficient to enable a spectral broadening, spreading from 0.6 to 4.1 μm in a 40 dB dynamic range.
Investigation of the Na2O/Ag2O ratio on the synthesis conditions and properties of the 80TeO2–10ZnO–[(10−x)Na2O–xAg2O] glasses
International audience; Properties of the tellurite glasses 80TeO2–10ZnO–[(10−x)Na2O–xAg2O] are investigated as a function of the substitution ratio x between Na2O and Ag2O. One observe that the variation of glass transition temperature decreases monotonously with x and that surface crystallization mechanism is favored. The assignment of the Raman bands and their relation with the underlying glass structure is discussed. While both Na2O and Ag2O oxides act as glass network modifiers, their progressive equimolar substitution does not lead to a meaningful evolution in the structure of the TZ[Na10-xAgx] glass. The refractive index and the cut-off wavelength are found to increase with x. The co…
Experimental investigation of Brillouin and Raman scattering in a 2SG sulfide glass microstructured chalcogenide fiber.
International audience; In this work, we investigate the Brillouin and Raman scattering properties of a Ge15Sb20S65 chalcogenide glass microstructured single mode fiber around 1.55 microm. Through a fair comparison between a 2-m long chalcogenide fiber and a 7.9-km long classical single mode silica fiber, we have found a Brillouin and Raman gain coefficients 100 and 180 larger than fused silica, respectively.
Core-clad phosphate glass fibers for biosensing
Recently, a phosphate glass with composition 20 CaO-20 SrO-10 Na2O-50 P2O5 (mol%) was found to have good potential as a biomaterial and to possess thermal properties suitable for fiber drawing. This study opened the path towards the development of fully bioresorbable fibers promising for biosensing. In the past, this phosphate glass with CeO2 was found to increase the refractive index and the glass stability. Therefore, a new SrO-containing glass was prepared with 1 mol% of CeO2 and core fibers were drawn from it. A core-clad fiber was also processed, where the core was a Ce-doped glass and the clad undoped, to allow for total internal reflection. The mechanical properties of the core and c…
Supercontinuum Generation in Tellurite Optical Fibers
This chapter presents a state of the art of infrared supercontinuum generation in heavy oxide tellurite optical fibers from the experimental results published by the international community. As a first part, a bibliographic table gathers the literature on which this work is based. Then, the second part briefly returns on the tellurite glass compositions, the third part presents the different fiber structures (microstructured, suspended core or step-index fibers, tapered fibers), the fourth part discusses the pumping sources in relation with the fiber chromatic dispersion as well as coupling issues, the supercontinuum performances are presented in the fifth part, and the sixth part deals wit…
Recent advances in chalcogenide holey fibres
oral
Mid-infrared 2000-nm bandwidth supercontinuum generation in suspended-core microstructured Sulfide and Tellurite optical fibers
International audience; In this work, we report the experimental observation of supercontinua generation in two kinds of suspended-core microstructured soft-glass optical fibers. Low loss, highly nonlinear, tellurite and As2S3 chalcogenide fibers have been fabricated and pumped close to their zero-dispersion wavelength in the femtosecond regime by means of an optical parametric oscillator pumped by a Ti:Sapphire laser. When coupled into the fibers, the femtosecond pulses result in 2000-nm bandwidth supercontinua reaching the Mid-Infrared region and extending from 750 nm to 2.8 mu m in tellurite fibers and 1 mu m to 3.2 mu m in chalcogenide fibers, respectively.
Chalcogenide Photonic Crystal Fibers for Near and Middle Infrared Applications
Chalcogenide glasses are based on sulphur, selenium, tellurium and the addition of other elements such as arsenic, germanium, antimony, gallium, etc. Chalcogenide fibers present numerous applications in the IR field, such as telecommunication at 1.55 mum, spectroscopy and military systems in the two atmospherics windows (3-5 mum and 8-12 mum). One of the interests of chalcogenide glasses is to associate high non linear properties with their Infrared transmission from 0.51 mum to 12-18 mum depending on the composition. Indeed, chalcogenide glasses present high third order optical properties, 100 - 1000 times as high as the non linearity of silica glass at 1.55 mum. For many applications, sin…
Optical aging behaviour naturally induced on As_2S_3 microstructured optical fibres
The efficiency and the stability of As2S3 microstructured optical fibres (MOFs) are limited by the shift of their optical properties that occurs over time due to a naturally induced aging process. Such sensitivity becomes more crucial for long optical path. Among the variety of fibre designs, the MOFs are developed for promising photonics applications such as supercontinuum generation for example. In the present work, we carried out an extensive aging study on As2S3 chalcogenide MOFs in ambient atmosphere. The evolution of the fibre transmission spectrum has been studied with regards to exposure time. The analysis of the transmission line profile was performed in terms of different spectral…
Mid-infrared supercontinuum generation in suspended-core chalcogenide and tellurite optical fibers
Summary form only given. The generation of optical supercontinua in the mid-infrared region and especially their expansion beyond the intrinsic limit dictated by fused silica is currently a subject of high interest. Tellurite and chalcogenide glasses have serious advantages because of their wide transmittance window which can reach more than 10 μm while the Kerr nonlinearity can be 500 times stronger than fused silica. These different features make them serious candidates for broad mid-infrared supercontinuum generation. For example, supercontinuum as broad as 4000-nm bandwidth has been generated in a sub-cm long Tellurite microstructured fiber by Domachuk et al. in ref. [1] by means of a f…
Te-As-Se glass microstructured optical fiber for the middle infrared
International audience; We present the first fabrication, to the best of our knowledge, of chalcogenide microstructured optical fibers in Te-As-Se glass, their optical characterization, and numerical simulations in the middle infrared. In a first fiber, numerical simulations exhibit a single-mode behavior at 3.39 and 9.3 μm, in good agreement with experimental near-field captures at 9.3 μm. The second fiber is not monomode between 3.39 and 9.3 μm, but the fundamental losses are 9 dB/m at 3:39 μm and 6 dB/m at 9.3 μm. The experimental mode field diameters are compared to the theoretical ones with a good accordance.
Chalcogenide microstructured optical fibers : from linear to nonlinear properties
International audience; In this talk, we review the linear properties of chalcogenide microstructured optical fibers (MOFs) of several types. We mainly focus our talk on mid-infrared applications of such fibers. We start with the general properties of solid core MOFs made of these high index glasses and compare them with the ones of silica. Then, we give some details concerning a solid core MOF made of TAS glass. Next, we describe the first guiding suspended chalcogenide MOF and explain how it was designed for supercontinuum generation in the mid-infrared. Both linear and nonlinear properties of As2S3 suspended core MOFs are also numerically studied. In the next part, We describe the design…
Management of OH absorption in tellurite optical fibers and related supercontinuum generation
Abstract We report the fabrication and the characterization of low OH content and low loss tellurite optical fibers. The influence of different methods of glass fabrication on fiber losses has been investigated. The use of the purest commercial raw materials can reduce the losses below 0.1 dB/m at 1.55 μm. Incorporation of fluoride ions into the tellurite glass matrix makes the optical fibers transparent up to 4 μm. A suspended core microstructured fiber has been fabricated and pumped by nanojoule-level femtosecond pulses, thus resulting in more than 2000-nm bandwidth supercontinuum after a few centimeters of propagation.
Suspended core tellurite glass optical fibers for infrared supercontinuum generation
International audience; We report the fabrication and characterization of tellurite TeO(2)-ZnO-Na(2)O (TZN) microstructured suspended core optical fibers (MOFs). These fibers are designed for infrared supercontinuum generation with zero dispersion wavelength (ZDW) at 1.451 mu m. The measured losses at this wavelength are approximately 6 dB/m for a MOF with a 2.2 mu m diameter core. The effective area of a particular fiber is 3.5 mu m(2) and the nonlinear coefficient is calculated to be 437 W(-1)km(-1). By pumping a 20 cm long fiber at 1.56 mu m with a sub-nj femtosecond laser source, we generate a supercontinuum (SC) spanning over 800 nm in the 1-2 mu m wavelength range.
Microstructured chalcogenide optical fibers from As2S3 glass: towards new IR broadband sources
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