Structural and Vibrational Properties of Corundum-type In2O3 Nanocrystals under Compression

6533b7d8fe1ef96bd126b88f

RESEARCH PRODUCT

Structural and Vibrational Properties of Corundum-type In2O3 Nanocrystals under Compression

D. Martinez-garcia B. García-domene Rosario Vilaplana D. Errandonea Vanesa P. Cuenca-gotor Plácida Rodríguez-hernández Julio Pellicer-porres Juan Angel Sans Anshu Singhal Francisco Javier Manjón Alfonso Muñoz Srungarpu N. Achary Catalin Popescu

subject

Materials science Corundum nanocrystals Thermodynamics Bioengineering Corundum Nanotechnology 02 engineering and technology engineering.material 010402 general chemistry Espectroscopia 01 natural sciences Indium oxide symbols.namesake Phase (matter)Nanocristales General Materials Science Electrical and Electronic Engineering highpressure Mechanical Engineering Difracción de rayos X General Chemistry 021001 nanoscience & nanotechnology Nanocrystalline material 0104 chemical sciences X-ray diffraction Nanocrystal Mechanics of Materials FISICA APLICADA X-ray crystallography Raman spectroscopy symbols engineering Orthorhombic crystal system Ab initio calculations 0210 nano-technology Raman spectroscopy Raman scattering Alta presión

description

[EN] This work reports the structural and vibrational properties of nanocrystals of corundum-type In2O3 (rh-In2O3) at high pressures by using angle-dispersive x-ray diffraction and Raman scattering measurements up to 30 GPa. The equation of state and the pressure dependence of the Raman-active modes of the corundum phase in nanocrystals are in good agreement with previous studies on bulk material and theoretical simulations on bulk rh-In2O3. Nanocrystalline rh-In2O3 showed stability under compression at least up to 20 GPa, unlike bulk rh-In2O3 which gradually transforms to the orthorhombic Pbca (Rh2O3-III-type) structure above 12 14 GPa. The different stability range found in nanocrystalline and bulk corundum-type In2O3 is discussed.

year	journal	country	edition	language
2017-04-21

http://riull.ull.es/xmlui/handle/915/4535

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