Über Lichtreaktionen, XVIII: Photolyse von Benzazid in verschiedenen Reaktionsmedien und ihre Sensibilisierung

6533b81ffe1ef96bd1278e39

RESEARCH PRODUCT

Über Lichtreaktionen, XVIII: Photolyse von Benzazid in verschiedenen Reaktionsmedien und ihre Sensibilisierung

Joachim Dörges Gerhard Bauer Leopold Horner

subject

Inorganic Chemistry Chemistry Medicinal chemistry

description

Bei der Photolyse von Benzazid entsteht Benzoylimen, welches Wasser, Eisessig, Anilin und in Konkurrenz mit Wasser auch Dimethylsulfoxyd anlagert. Bei der thermischen Zersetzung wird kein Benzoylimen gebildet. — Photolytisch erzeugtes Benzoylimen liefert mit primaren und sekundaren Alkoholen a) Urethane (I), b) O-Alkyl-N-benzoyl-hydroxylamin-Derivate (II), c) Benzamid (III) neben Aldehyden bzw. Ketonen. — Bei der durch Benzophenon sensibilisierten Photolyse von Benzazid in Athanol bzw. Isopropylalkohol entstehen zu 100% Benzamid sowie Acetaldehyd bzw. Aceton.

year	journal	country	edition	language
1965-08-01	Chemische Berichte

https://doi.org/10.1002/cber.19650980831

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