Die Abtrennung geringster Mengen von Osmium und Ruthenium durch Destillation

6533b834fe1ef96bd129def9

RESEARCH PRODUCT

Die Abtrennung geringster Mengen von Osmium und Ruthenium durch Destillation

subject

Chemistry Clinical Biochemistry General Materials Science General Medicine Analytical Chemistry Nuclear chemistry

description

Die fur die Abtrennung von Osmium und Ruthenium gebrauchliche Destillation als Tetroxyde aus saurer, oxydierender Losung ist auch fur Mikrogramm-Mengen beider Elemente anwendbar. Nach Ermittlung der in diesem Bereich moglichen Fehlerquellen wird ein geeigneter Destillationsapparat beschrieben; es wird eine Arbeitsvorschrift fur die Destillation mit Chromsaure und Schwefelsaure bzw. Perchlorsaure gegeben, deren Zuverlassigkeit belegt wird. Metallmengen zwischen 5 und 100μg konnen auf 5–10% genau erfast werden.

year	journal	country	edition	language
1957-11-01	Fresenius' Zeitschrift für analytische Chemie

https://doi.org/10.1007/bf00592509

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