Search results for " Digestion"

ICP-MS multielement determination in fly ash after microwave-assisted digestion of samples.

2001

A microwave assisted digestion procedure has been developed for dissolution of fly ash samples prior to the inductively coupled plasma-mass spectrometric determination of their elemental composition. The developed methodology was validated by carrying out the analysis of two high-silicate containing reference materials (CRM 134R sewage amended soil and NIES JR 1 rock) and by means of the comparison between results found by microwave-assisted digestion and ICP-MS of fly ash samples with those found by neutron activation analysis (NAA) for Sb, Cs, Cr, Co, Fe, U and Zn determination. The method developed can be recommended for routine multielement analysis of fly ash.

An ultrasound-assisted digestion method for the determination of toxic element concentrations in ash samples by inductively coupled plasma optical em…

2007

Abstract A method of ultrasound-assisted digestion followed by inductively coupled plasma optical emission spectrometry (ICP-OES) used for the determination of toxic element concentrations (arsenic, barium, cobalt, copper, lead, nickel, strontium, vanadium and zinc) in ash samples was developed. All the measurements were performed in robust plasma conditions which were tested by measuring the Mg(II) 280.270 nm/Mg(I) 285.213 nm line intensity ratios. The highest line intensity ratios were observed when a nebulizer gas flow of 0.6 L min−1, auxiliary gas flow of 0.2 L min−1 and plasma power of 1400 W were used for radially viewed plasma. The analysis of SRM 1633b showed that the ultrasound-ass…

Determination of chromium in foods by flame atomic absorption and inductively coupled plasma spectrometry

1989

Sicilian potential biogas production from Citrus industry by-product

2017

In Europe, Italy is the second nation after Spain in Citrus production and 49% ca. of national fruit production is located in Sicily. The by-product obtained from the industrial processing of Citrus fruits into juice and essential oils is called “pastazzo” or Citrus Waste (CW). This study is aimed at evaluating the Sicilian potential biogas and energy production from the above “pastazzo” and verifying the possibility of using this by-product for Anaerobic Digestion (AD) process within 30 km from processing plants. The areas cultivated with Citrus species in Sicily and their distribution in the various municipal districts were mapped and analysed by means of QGIS software, together with the …

Influence of orange cultivar and mandarin postharvest storage on polyphenols, ascorbic acid and antioxidant activity during gastrointestinal digestio…

2017

Polyphenols, ascorbic acid content and antioxidant activity of two sweet oranges (Navel-N and Cara Cara-CC) and mandarin (Clementine-M) as well as their bioaccessibilities were evaluated in pulps and compared to those in fresh juice. Thus, pulps of oranges and mandarins displayed higher hesperidin (HES), narirutin (NAR), total flavonoids (TF), total phenols (TP) and antioxidant activity (AAC) than their corresponding juices. Also, CC products presented higher bioactive compounds content than N ones. Bioaccessibility of bioactive compounds and AAC were higher in pulps of both oranges and mandarin than in their corresponding juices. Oranges (N and CC) pulps and juices presented higher bioacce…

Effects of temperature on post-methanation of digested dairy cow manure in a farm-scale biogas production system.

2003

A post-methanation process that could be adopted at farm-scale, operating at temperatures prevailing in farm manure digester post-storage tanks, was evaluated. Digested manure samples from a farm digester (35 degrees C) and post-storage tank (5-10 degrees C) were incubated in parallel batches at 5-20 degrees C and as reference at 35 and 55 degrees C. Specific methane yields (kg(-1) volatile solids (VS)(added waste)) were 0.20-0.26 m3 at 35-55 degrees C and 0.085-0.09 m3 at 10-20 degrees C for digester material (345 days of incubation) and 0.16-0.21 m3 at 35-55 degrees C, 0.053-0.087 kg(-1) VS(added waste) m3 at 15-20 degrees C and 0.026 m3 at 10 degrees C for post-storage tank material (250…

Assessment of the Energy Potential of Chicken Manure in Poland

2019

Animal waste, including chicken manure, is a category of biomass considered for application in the energy industry. Poland is leading poultry producer in Europe, with a chicken population assessed at over 176 million animals. This paper aims to determine the theoretical and technical energy potential of chicken manure in Poland. The volume of chicken manure was assessed as 4.49 million tons per year considering three particular poultry rearing systems. The physicochemical properties of examined manure specimens indicate considerable conformity with the data reported in the literature. The results of proximate and ultimate analyses confirm a considerable effect of the rearing system on the e…

Storing energy crops for methane production: Effects of solids content and biological additive

2007

The effect of storage on chemical characteristics and CH4 yield (taking into account loss of VS during storage) of a mixture of grasses and ryegrass, ensiled as such (low solids content) and after drying (medium and high solids) with and without biological additive, were studied in field and laboratory trials. Up to 87% and 98% of CH4 yield was preserved with low solids grass (initial TS 15.6%) and high solids ryegrass (initial TS 30.4%), respectively, after storage for 6months, while under suboptimal conditions at most 37% and 52% of CH4 yield were lost. Loss in CH4 yield was mainly due to VS loss, presumably caused by secondary fermentation as also suggested by increasing pH during storag…

Impact of crop species on bacterial community structure during anaerobic co-digestion of crops and cow manure

2008

The bacterial communities in three continuously stirred tank reactors co-digesting cow manure with grass silage, oat straw, and sugar beet tops, respectively, were investigated by 16S rRNA gene-based fingerprints and clone libraries. The analyses revealed both clearly distinct and similar phylotypes in the bacterial communities between the reactors. The major groups represented in the three reactors were Clostridia, unclassified Bacteria, and Bacteroidetes. Phylotypes affiliated with Bacilli or Deltaproteobacteria were unique to the sugar beet and straw reactor, respectively. Unclassified Bacteria dominated in sugar beet reactor while in the straw and grass reactor Clostridia was the domina…

Hydrolysis and microbial community analyses in two-stage anaerobic digestion of energy crops

2007

Aims: The roles of the diverse populations of micro-organisms responsible for biodegradation of organic matter to form methane and carbon dioxide are rudimentarily understood. To expand the knowledge on links between microbial communities and the rate limiting, hydrolytic stage of two-stage biogas production from energy crops, this study was performed. Methods and Results: The process performance. and microbial communities (as determined by fluorescence in situ hybridization) in two separate two-stage batch digestions of sugar beets and grass/clover were studied. The microbial populations developed in the hydrolytic stage of anaerobic digestion of beets and grass/clover showed very few simi…