Search results for " GC"
showing 10 items of 86 documents
Influence of "single-origin" coffees on sensory characteristics of Espresso.
2004
Evaluation of matrix effect on the GC/MS response of eighteen pesticides by multivariate approach
2015
IDENTIFICAZIONE CON GC/MS E INDAGINE MICROBIOLOGICA DI POLLO IRRADIATO
2005
Caratterizzazione delle vernici utilizzate nella liuteria storica
2009
Selection of sampling adsorbents and optimisation and validation of a GC-MS/MS method for airborne pesticides
2017
ABSTRACTA methodology for the sampling and determination of airborne pesticides has been developed. The trapping efficiency of three adsorbents, namely XAD-2,XAD-4 and a sandwich sorbent (PUF-XAD2-PUF), was tested for 34 pesticides and the latter was selected because it presented the highest retention capacity without breakthrough. Pesticides were determined by gas chromatography coupled to an ion trap mass spectrometer in tandem. The method showed recoveries ranging from 70% to 120% with limits of quantification in the range of 16.1–322.6 pg m−3 when 155 m3 were sampled. This analytical strategy was applied to 10 indoor air samples collected in dwellings from the Valencian Region. Six pest…
Chemical composition of the essential oil from aerial parts of Stachys palustris L. (Lamiaceae) growing wild in Southern Italy
2007
The paper reports the composition of the essential oil from aerial parts of Stachys palustris L. (Lamiaceae) from Southern Italy. The essential oil was extracted by hydrodistillation from selected plants and its chemical composition was determined by the GC-MS system on two fused- silica capillary columns of different polarity. The mass fraction of oil was 0.21 % on a dry weight basis. Altogether, 92 compounds were identified accounting for 93.6 % of the total oil, which was characterized mainly by carbonylic compounds (25.4 %), fatty acids and their esters (24.2 %), along with sesquiterpenoidic compounds (16.0 %) and phenols (11.2 %). The major components of the sample were caryophyllene o…
Characterization of Leaf Essential Oil Composition of Homozygous and HeterozygousCitrus clementinaHort. Extan. and its Ancestors
2013
Clementine is a natural tangor, resulting from an interspecific cross between mandarin and sweet orange. Gametic embryogenesis, allowing the single-step development of complete homozygous line from the heterozygous parents, increases the efficiency of perennial crop breeding programs. Tri-haploids have been regenerated through pollen embryogenesis (specifically, by anther culture) of Citrus clementina Hort. ex Tan., cv. Nules. Two of them (HOMO1 and HOMO2) have been acclimatized and grafted in vivo in 2000. Research regarding the chemical characteristics of plant regenerated by pollen embryogenesis or gynogenesis are useful to study the “gametoclonal variation”, as well as for further appli…
Structural Characterisation of Complex Layered Double Hydroxides and TGA-GC-MS Study on Thermal Response and Carbonate Contamination in Nitrate- and …
2015
Layered double hydroxides (LDHs) are versatile materials used for intercalating bioactive molecules in the fields of pharmaceuticals, nutraceuticals and cosmetics, with the purpose of protecting them from degradation, enhancing their water solubility to increase bioavailability and improving their pharmacokinetic properties and formulation stability. Moreover, LDHs are used in various technological applications to improve stability and processability. The crystal chemistry of hydrotalcite-like compounds was investigated by X-ray powder diffraction (XRPD), automated electron diffraction tomography (ADT) and thermogravimetric analysis (TGA)-GC-MS to shed light on the mechanisms involved in io…
Confronto chemiotipico tra accessioni spontanee e coltivate del genere Thymus raccolte sui monti Nebrodi (Sicilia N-E)
2009
Il genere Thymus, largamente rappresentato all'interno della flora spontanea mediterranea, comprende numerose specie tradizionalmente adoperate dalle popolazioni residenti nel comprensorio, che ne fanno uso per svariate finalità alimentari, medicinali e artigianali. Per questo motivo numerosi timi, oltre che prelevati dallo spontaneo, vengono anche tradizionalmente coltivati all'interno di giardini e orti domestici, che presumibilmente avranno giocato un ruolo importante nelle dinamiche di differenziazione e conservazione delle specie. Con l'obiettivo di acquisire nuove informazioni in tal senso, nella primavera-estate del 2007 accessioni di Thymus spinulosus e Thymus longicaulis sono state…
Comparison of the volatile oils ofHypericum scabrum L. andHypericum perforatum L. from Turkey
1997
The composition of the volatile oils obtained from the aerial parts of Hypericum scabrum L. and H. perforatum L. was analysed by GC and GC‐MS. While the oil of H. scabrum L. contained a-pinene (71.6%), b-caryophyllene (4.8%), myrcene (3.8%), cadalene (3.4%) and b-pinene (2.9%), the oil of H. perforatum L. contained a-pinene (61.7%), 3-carene (7.5%), b-caryophyllene (5.5%), myrcene (3.6%), cadalene (3.2%) and other components. Twenty-nine and 27 terpenoid compounds have been identified in the volatile oils of H. scabrum L. and H. perforatum L., respectively. #1997 by John Wiley & Sons, Ltd.