Search results for "Instrumentation"
showing 10 items of 4914 documents
A stochastic shape and orientation model for fibres with an application to carbon nanotubes
2012
Methods are introduced for analysing the shape and orientation of planar fibres from greyscale images of fibrous systems. The sequence of image processing techniques needed for segmentation of fibres is described. The identified fibres were interpreted as deformed line segments for which two shape and two orientation parameters are estimated by the maximum likelihood method. The methods introduced are shown to perform quite well for simulated systems of deformed line segments with known properties. They were applied to TEM images of carbon nanotubes embedded in polycarbonate.
Determination of Bubble Size Distribution Using Ultrasound Array Imaging
2020
In this article, ultrasonic phased arrays are deployed as an imaging tool for industrial process analysis. Such arrays are typically used for sonar, medical diagnosis, and nondestructive testing; however, they have not yet been applied to industrial process analysis. The precise positioning of array elements and high frequencies possible with this technology mean that highly focused images can be generated, which cannot currently be achieved using ultrasound tomography. This article aims to highlight the potential of this technology for the measurement of bubble size distribution (BSD) and to demonstrate its application to both intrusive and noninvasive process measurements. Ultrasound imag…
Cladding-Pumped Erbium/Ytterbium Co-Doped Fiber Amplifier for C-Band Operation in Optical Networks
2021
Space-division multiplexing (SDM) attracts attention to cladding-pumped optical amplifiers, but they suffer from a low pump power conversion efficiency. To address this issue, ytterbium (Yb3+) and erbium (Er3+) co-doping is considered as an effective approach. However, it changes the gain profile of Er3+-doped fiber amplifiers and induces the gain difference between optical wavelengths in the C-band, significantly limiting the effective band of the dense wavelength-division multiplexed (DWDM) system. This paper is devoted to a detailed study of a cladding-pumped Er3+/Yb3+ co-doped fiber amplifier (EYDFA) through numerical simulations aiming to identify a configuration, before assembling a s…
Thermostimulated luminescence of plasma electrolytic oxidation coatings on 6082 aluminium surface
2019
Financial support provided by Scientific Research Project for Students and Young Researchers Nr. SJZ/2016/12 realized at the Institute of Solid State Physics, University of Latvia is greatly acknowledged. Authors are grateful to R. Ignatans for measurements and analysis of XRD spectra and ElGoo Tech ltd. for providing PEO equipment.
Energy resolution and throughput of a new real time digital pulse processing system for x-ray and gamma ray semiconductor detectors
2013
New generation spectroscopy systems have advanced towards digital pulse processing (DPP) approaches. DPP systems, based on direct digitizing and processing of detector signals, have recently been favoured over analog pulse processing electronics, ensuring higher flexibility, stability, lower dead time, higher throughput and better spectroscopic performance. In this work, we present the performance of a new real time DPP system for X-ray and gamma ray semiconductor detectors. The system is based on a commercial digitizer equipped with a custom DPP firmware, developed by our group, for on-line pulse shape and height analysis. X-ray and gamma ray spectra measurements with cadmium telluride (Cd…
Non-destructive technique to detect local buried defects in metal sample by scanning microwave microscopy
2012
International audience; Based on the skin effect, our recent developments using scanning microwave microscopy lead to propose a non-destructive method to detect located buried defect in metal samples like stainless steel. A 3D tomography is possible by taking advantage of microwave measurement, using a vector network analyzer in bandwidth frequencies, and the nanometer resolution positioning capabilities with atomic force microscopy. At each used frequency, an incident electromagnetic wave is sent to the sample and the reflected wave gives information on a specific depth layer in the material. With diagnostic tools of nanotechnologies (SEM. AFM, etc.), different stainless steel samples (fro…
Hybrid electrochemical/electrochromic Cu(II) ion sensor prototype based on PANI/ITO-electrode
2017
Abstract Conducting polymer polyaniline (PANI) based electrochromic films were electrochemically synthesized on indium tin oxide (ITO) covered glass electrodes and their electrochromic performances were investigated by spectroscopic methods before and after the incubation in Cu(II) ion containing aqueous solution. Chemical structure of synthesized PANI layer was evaluated by FTIR. The electrochromic performance of PANI film was determined by measuring of spectroscopic signals before and after the incubation of PANI film coated electrode in Cu(II) ion containing solution. During the change of potential, which was applied to PANI-modified electrode, the colour of PANI thin film turned from gr…
Measurements of thickness dispersion in biolayers by scanning force microscopy and comparison with spectroscopic ellipsometry analysis.
2007
Measuring the thickness of biological films remains a difficult task when using differential measurements by atomic force microscopy (AFM). The use of microstructured substrates combined with a selective adsorption constitutes an alternative to tribological measurements. The statistical thickness analysis of biological layers, especially via the dispersion measurements, can provide a way to quantify the molecular orientation. AFM thicknesses were then compared with those obtained optically by spectroscopic ellipsometry (SE) and surface plasmon resonance enhanced ellipsometry (SPREE). The biolayers could then be modeled using a vertical gradient of optical index, which reflects height disper…
Benzene monitoring by micro-machined sensors with SnO2 layer obtained by using micro-droplet deposition technique
2011
International audience; SnO2 thin layers were deposited by the way of the micro-droplet technique. The sensor substrate consisted of a thin membrane developed on oxidised silicon wafer. The sensing layers were deposited by means of the micro-droplet technique into thin layers of about 100 nm. Such devices were tested for benzene detection. The obtained results showed a very high sensitivity for this chemical compound since 500 ppb were detected. The results presented in this paper were not focused on the reactional mechanism of benzene detection but rather on the development of a cheap and sensitive sensor using sol-gel and micro-droplet processes. Since these layers were elaborated using s…
A nanostructured sensor of hydrogen peroxide
2017
Abstract A nanostructured electrochemical sensor of hydrogen peroxide was fabricated growing self-standing Pd nanowires (Pd NWs) into polycarbonate (PC) membranes through a simple metal galvanic deposition. Conditions of deposition were adjusted in order to attain 2–5 μm long Pd wires. Characterization of Pd-NWs was performed by scanning electrode microscopy, energy-dispersive X-ray spectroscopy and X-ray diffraction. Properties of the nanostructured sensor were studied by cyclic voltammetry and chronoamperometry in phosphate buffer—ethanol solution. Addition of pure ethanol to the test solution was essential in order to increase wettability of the nanostructures. Sensing features were comp…