Search results for "performance"
showing 10 items of 4457 documents
High-performance liquid chromatographic, capillary electrophoretic and capillary electrophoretic–electrospray ionisation mass spectrometric analysis …
2002
Systems for efficient separation of selected alkaloid groups by high performance liquid chromatography (HPLC), capillary electrophoresis (CE) and capillary electrophoresis coupled with electrospray ionisation mass spectrometry (CE-ESI-MS) are described. The optimized HPLC system was applied for the separation of 23 standard indole alkaloids as well as for qualitative and quantitative analyses of crude alkaloid extracts of Rauvolfia serpentina X Rhazya stricta hybrid cell cultures. The developed conditions for CE analysis proved to be efficient for separation of mixtures of standard indole and beta-carboline alkaloids. The described buffer system is also applicable in the combination of CE w…
Development of an efficient system for the separation of indole alkaloids by high performance liquid chromatography and its applications
2001
An efficient system for the analysis of indole alkaloids by HPLC on a reversed-phase column using an ion pair technique is described. The optimised chromatographic conditions allowed the successful separation of 22 standard monoterpenoid indole alkaloids (including some isomers) and tryptamine. The described HPLC system was applied to the analysis of alkaloids in intergeneric somatic hybrid cell cultures of Rauvolfia serpentina x Rhazya stricta.
Screening of oxazepine indole enantiomers by means of high performance liquid chromatography with imprinted polymer stationary phase.
2004
Chromatographic enantiomer separations of different oxazepine indole derivatives were performed using a molecularly imprinted polymer. A 5aR,12R,13S-trans-6,6-dimethyl-12,13-dihydro-6H-5a, 1 3-methanoindolo[2,1-b][1,3]naphthoxazepine-12-carboxamide enantiomerderivative was used as a template and the resultant polymer has shown enantiomer recognition for series of template related compounds. The mechanistic description of the chiral discrimination process is scrutinised, comparing the discrimination between the different conformations and substituents of the oxazepine indoles.
Relation between anaerobic power and rowing ergometer performance in young rowers
2013
Aims: Rowing performance over 2000m is dependent upon the functional capacity of both the aerobic and anaerobic energy pathways. Although several studies have indicated that maximal oxygen uptake is strongly related to rowing performance and it is the best predictor of performance in elite rowers, some evidence is that muscle power output could be an important predictor of performance. The aim of this study was to investigate the possible relationship between anaerobic power and rowing ergometer performance over 2000m in young rowers, and whether anaerobic power assessed could identify athletes with the best performance. Methods: We collected biometric characteristics and energy data, inclu…
Determination of phenolic antioxidants additives in industrial wastewater from polypropylene production using solid phase extraction with high-perfor…
2019
Abstract This paper describes a new method for the effective extraction of the residues of five synthetic phenolic antioxidants (AOs): Ditertbutylphenol (DTF), Irganox 1010, Irganox 1076, Ethanox 330 and Cyanox 1790, from industrial water produced during the polypropylene (PP) deodorization process. In the deordorization process, PP is stored in a column for an average time of four hours and exposed to nitrogen and water vapor to remove inflammable compounds which may generate atypical odors in the PP. The samples of interest were taken in the desorber, followed by cleansing and pre-concentration using modified styrene divinylbenzene polymer cartridges. Liquid chromatography was performed w…
Some New Symbolic Algorithms for the Computation of Generalized Asymptotes
2022
We present symbolic algorithms for computing the g-asymptotes, or generalized asymptotes, of a plane algebraic curve, C, implicitly or parametrically defined. The g-asymptotes generalize the classical concept of asymptotes of a plane algebraic curve. Both notions have been previously studied for analyzing the geometry and topology of a curve at infinity points, as well as to detect the symmetries that can occur in coordinates far from the origin. Thus, based on this research, and in order to solve practical problems in the fields of science and engineering, we present the pseudocodes and implementations of algorithms based on the Puiseux series expansion to construct the g-asymptotes of a p…
Applying system dynamics to foster organizational change, accountability and performance in the public sector: A case-based Italian perspective
2010
The goal of this paper is to discuss the role System Dynamics (SD) can play to enhance performance improvement in the public sector. It is remarked how SD can help decision makers to properly perceive the boundaries of the relevant system underlying observed phenomena. To this end, three real cases are analysed to show how SD can facilitate a better understanding of the relationships between the political and the organisational system in the public sector, and how to promptly attain efficiency and improve outcome, given the constraints that the institutional and political systems constitute. The goal of this paper is to discuss the role System Dynamics (SD) can play to enhance performance i…
Assessing the Effect of the Economy for the Common Good System on Business Performance
2023
Extant literature has pointed to organizational hybridity to lever sustainable business transformation. Moreover, some authors hold that there is a possible trade-off between sustainability and performance. However, there is still little empirical evidence on the impact that such sustainability-driven hybridization systems have on performance. Thus, the present study’s main goal is to fill this gap by providing empirical evidence on the impact of the implementation of the Economy for the Common Good, as a sustainability-driven organizational system, on business performance. To do so, the authors relied on a sample of 206 businesses from five European countries. Then, the authors follo…
The real-life performance of market timing with moving average and time-series momentum rules
2014
In this article, we revisit the myths regarding the superior performance of market timing strategies based on moving average and time-series momentum rules. These active timing strategies are very appealing to investors because of their extraordinary simplicity and because they promise substantial advantages over their passive counterparts. However, the ‘too good to be true’ reported performance of these market timing rules raises a legitimate concern as to whether this performance is realistic and whether investors can expect that future performance will be the same as the documented historical performance. We argue that the reported performance of market timing strategies usually contains…
Dealing with Multi-Level Governance and Wicked Problems in Urban Transportation Systems: The Case of Palermo Municipality
2015
Italian New Public Management (NPM) has been mainly characterized by a political orientation toward power decentralization to local governments and privatization of public companies. Nowadays, local utilities in Italy are often run by joint stock companies controlled by public agencies such as Regional and Municipal Administrations. Due to this transformation, these companies must comply with a set of diverse expectations coming from a wide range of stakeholders, related to their financial, competitive and social performance. Such fragmented governance increases the presence of “wicked” problems in the decision-making sphere of these entities. Given this multi-level governance structure, ho…