Search results for "techniques"

showing 10 items of 4426 documents

Relation between bone quality values from ultrasound transmission velocity and implant stability parameters--an ex vivo study.

2011

Aim The objective of this study was to determine the relationship between bone qualities measured by ultrasound transmission velocity (UTV) and primary implant stability parameters measured by radiofrequency analysis (RFA) and push-out test (POT) in an ex-vivo model. Materials and methods Three blocks of fresh porcine bone samples were obtained from different anatomic regions, correlating to cortical, mixed and cancellous bone. Mechanical bone qualities of these samples were measured using UTV (expressed in m/s) prior to implantation. Three similar implants (4.1 × 11 mm, AstraTech OS) were inserted into each of the procured bone blocks. The evaluation of implant-bone interface stability was…

Materials scienceRadio WavesSwineDentistryIn Vitro TechniquesDental Prosthesis RetentionIliumImplants ExperimentalPorcine boneBone qualitymedicineAnimalsUltrasonographyDental ImplantsTibiabusiness.industryUltrasoundDental Implantation EndosseousImplant stability quotientmedicine.anatomical_structureModels AnimalImplantOral SurgerybusinessCancellous boneEx vivoBiomedical engineeringClinical oral implants research
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Microhardness of different resin cement shades inside the root canal

2012

Objectives: To compare microhardness along the root canal post space of two resin cements in different shades and a dual-cure resin core material. Study Design: Root canals of 21 bovine incisors were prepared for post space. Translucent posts (X•Post, Dentsply DeTrey) were luted using one the following resin luting agent: Calibra (Dentsply DeTrey) in Translucent, Medium and Opaque shades, RelyX Unicem (3M ESPE) in Translucent, A2 and A3 shades and the dual-cure resin core material Core•X flow. All materials were applied according to manufacturers’ instructions and were all photopolymerized (Bluephase LED unit, Ivoclar Vivadent, 40s). After 24 hours, roots were transversally cut into 9 slice…

Materials scienceRelyX UnicemRoot canalDentistryIn Vitro TechniquesIndentation hardnessClinical and Experimental DentistryMaterials TestingmedicineAnimalsHardness TestsGeneral DentistryResin cementCementDental Pulp Cavitybusiness.industryLuting agent:CIENCIAS MÉDICAS [UNESCO]Resin Cementsmedicine.anatomical_structureOtorhinolaryngologyUNESCO::CIENCIAS MÉDICASResearch-ArticleCattleSurgeryAdhesiveDental Pulp Cavitybusiness
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Using the simplified falling head technique to detect temporal changes in field-saturated hydraulic conductivity at the surface of a sandy loam soil

2007

Abstract Determining temporal changes in field-saturated hydraulic conductivity ( K fs ) is important for understanding and modeling hydrological phenomena at the field scale. Little is known about temporal variability of K fs values measured at permanent sampling points. In this investigation, the simplified falling head (SFH) technique was used for an approximately 2-year period to determine temporal changes in K fs at 11 permanent sampling points established at the surface of a sandy loam soil. Additional K fs measurements were obtained by the single-ring pressure infiltrometer (PI) technique to also compare the SFH and PI techniques. The lowest mean values of K fs , M ( K fs ), were det…

Materials scienceRepeated samplingHydrostatic pressureAnalytical chemistrySoil ScienceMineralogyTemporal variabilitySaturated hydraulic conductivityHydraulic conductivityDry soilLoamMeasurement techniquesSoil waterSettore AGR/08 - Idraulica Agraria E Sistemazioni Idraulico-ForestaliInfiltrometerAgronomy and Crop ScienceEarth-Surface Processes
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Evaluation of mechanical and morphologic features of PLLA membranes as supports for perfusion cells culture systems

2015

Abstract Porous biodegradable PLLA membranes, which can be used as supports for perfusion cell culture systems were designed, developed and characterized. PLLA membranes were prepared via diffusion induced phase separation (DIPS). A glass slab was coated with a binary PLLA–dioxane solution (8 wt.% PLLA) via dip coating, then pool immersed in two subsequent coagulation baths, and finally dried in a humidity-controlled environment. Surface and mechanical properties were evaluated by measuring pore size, porosity via scanning electron microscopy, storage modulus, loss modulus and loss angle by using a dynamic mechanical analysis (DMA). Cell adhesion assays on different membrane surfaces were a…

Materials scienceScanning electron microscopePolyestersCell Culture TechniquesPolyesterBioengineeringNanotechnology02 engineering and technologyCondensed Matter Physic010402 general chemistry01 natural sciencesDip-coatingCell LineBiomaterialsElastic ModulusTensile StrengthDynamic modulusHumansMechanics of MaterialPorosityElastic modulusMechanical PhenomenaElastic ModuluEpithelial CellMechanical Engineeringtechnology industry and agricultureTemperatureCell adhesionEpithelial CellsMembranes ArtificialDynamic mechanical analysis021001 nanoscience & nanotechnology0104 chemical sciencesPLLA membranePolyesterPerfusionMembraneChemical engineeringMechanics of MaterialsMaterials Science (all)Stress Mechanical0210 nano-technologyMechanical propertieCell Culture TechniquePorosityHuman
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Heavy-ion induced single event effects and latent damages in SiC power MOSFETs

2022

The advantages of silicon carbide (SiC) power MOSFETs make this technology attractive for space, avionics and high-energy accelerator applications. However, the current commercial technologies are still susceptible to Single Event Effects (SEEs) and latent damages induced by the radiation environment. Two types of latent damage were experimentally observed in commercial SiC power MOSFETs exposed to heavy-ions. One is observed at bias voltages just below the degradation onset and it involves the gate oxide. The other damage type is observed at bias voltages below the Single Event Burnout (SEB) limit, and it is attributed to alterations of the SiC crystal-lattice. Focused ion beam (FIB) and s…

Materials scienceScanning electron microscopeRadiationFocused ion beamelektroniikkakomponentitIonSEEschemistry.chemical_compoundstomatognathic systempuolijohteetGate oxideSilicon carbideSiC MOSFETsHeavy-ionDetectors and Experimental TechniquesElectrical and Electronic EngineeringPower MOSFETSafety Risk Reliability and Qualitybusiness.industryionisoiva säteilyCondensed Matter PhysicsLatent damageAtomic and Molecular Physics and OpticsSurfaces Coatings and FilmsElectronic Optical and Magnetic MaterialssäteilyfysiikkachemistrytransistoritOptoelectronicsSiC MOSFETs; Heavy-ion; Latent damage; SEEsbusinessVoltageMicroelectronics Reliability
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High-density polyethylene facial implants show surface oxidation in SEM and EDX examination: a pilot study.

2009

Previous histopathological studies on explanted Medpor high-density polyethylene (HDPE) facial implants indicated signs of material destruction and claimed to observe phagocytized HDPE particles within the tissue samples beside the usual type IV reaction with severe fibrosis. We examined new and explanted Medpor material with scanning electron microscopy (SEM) and energy-dispersive X-ray analysis (EDX). The implant surface of three patient-derived specimens showed significantly higher oxygenation in EDX analysis and morphological changes in SEM compared to the new unused material directly after opening of the package and after 1 year of exposure to air. Our preliminary findings indicate a p…

Materials scienceScanning electron microscopeSurface PropertiesBiomedical EngineeringPilot ProjectsSurgical implantsSevere fibrosisBiochemistryChemistry Techniques AnalyticalBiomaterialschemistry.chemical_compoundUsual typeSurface oxidationComposite materialMolecular BiologyX-RaysGeneral MedicineProstheses and ImplantsPolyethylenechemistryPolyethyleneMicroscopy Electron ScanningHigh-density polyethyleneImplantOxidation-ReductionBiotechnologyActa biomaterialia
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Study of silica-based intrinsically emitting nanoparticles produced by an excimer laser

2019

International audience; We report an experimental study demonstrating the feasibility to produce both pure and Ge-doped silica nanoparticles (size ranging from tens up to hundreds of nanometers) using nanosecond pulsed KrF laser ablation of bulk glass. In particular, pure silica nanoparticles were produced using a laser pulse energy of 400 mJ on pure silica, whereas Ge-doped nanoparticles were obtained using 33 and 165 mJ per pulse on germanosilicate glass. The difference in the required energy is attributed to the Ge doping, which modifies the optical properties of the silica by facilitating energy absorption processes such as multiphoton absorption or by introducing absorbing point defect…

Materials scienceScanning electron microscopemedicine.medical_treatmentAnalytical chemistryPhysics::OpticsGeneral Physics and AstronomyNanoparticleCathodoluminescenceCondensed Matter02 engineering and technologylcsh:Chemical technologylcsh:Technology01 natural sciencesFull Research PaperNanomaterials010309 opticsoptical materials0103 physical sciencesScanning transmission electron microscopymedicineNanotechnologylcsh:TP1-1185General Materials ScienceDetectors and Experimental TechniquesElectrical and Electronic Engineeringlcsh:Sciencenanomaterials[PHYS.PHYS.PHYS-OPTICS]Physics [physics]/Physics [physics]/Optics [physics.optics]Laser ablationExcimer laserlcsh:TGe-dopedSilica021001 nanoscience & nanotechnologyNanomateriallcsh:QC1-999Laser ablationAmorphous solidNanoscienceOptical materiallcsh:Q0210 nano-technologylcsh:Physics
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The rapid anastomosis between prevascularized networks on silk fibroin scaffolds generated in vitro with cocultures of human microvascular endothelia…

2010

The survival and functioning of a bone biomaterial upon implantation requires a rapidly forming and stably functioning vascularization that connects the implant to the recipient. We have previously shown that human microcapillary endothelial cells (HDMEC) and primary human osteoblast cells (HOS) in coculture on various 3-D bone biomaterial scaffolds rapidly distribute and self-assemble into a morphological structure resembling bone tissue. Endothelial cells form microcapillary-like structures containing a lumen and these were intertwined between the osteoblast cells and the biomaterial. This tissue-like self-assembly occurred in the absence of exogenously added angiogenic stimuli or artific…

Materials scienceSilkBiophysicsFibroinBiocompatible MaterialsBioengineeringBone tissueBone and BonesBiomaterialsMiceIn vivomedicineAnimalsHumansInosculationMicrovesselCells CulturedOsteoblastsTissue EngineeringTissue ScaffoldsfungiEndothelial CellsBiomaterialOsteoblastCoculture TechniquesCell biologyEndothelial stem cellmedicine.anatomical_structureMechanics of MaterialsCeramics and CompositesFemaleFibroinsBiomedical engineeringBiomaterials
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Improvement of the butyl methacrylate-paraffin embedment.

1983

The excellent butyl methacrylate-paraffin method as an embedment for light microscopy has been technically improved. More uniform and reproducible polymerization has been obtained by using a vacuum oven to degas the polymerizing mixture and to replace the air with nitrogen at 650 Torr. The amount of benzoyl peroxide required must be determined for each batch of butyl methacrylate. A teflon lined, reusable metal mold and a method of one-step blocking of tissues in preparation for sectioning are also described.

Materials scienceStaining and LabelingEmbedmentHistological Techniquestechnology industry and agriculturechemistry.chemical_elementBenzoyl peroxideNitrogenButyl methacrylateVacuum furnaceFixativeschemistryChemical engineeringPolymerizationPolymethacrylic AcidsParaffinTorrPolymer chemistryMicroscopymedicineMethacrylatesAnatomymedicine.drugStain technology
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Phonons of hexagonal BN under pressure: Effects of isotopic composition

2021

Raman scattering experiments on isotopically enriched hexagonal boron nitride have been performed under pressure up to 11 GPa at room temperature. The sublinear increase of the Raman-active E2g mode frequencies has been characterized. The pressure behavior has been analyzed by means of a bond-stiffness–bond-length scaling parameter γ which takes into consideration the vast differences in a- and c-axis compressibilities. The interlayer shear mode exhibits a γ parameter similar to that of graphite, and the mode frequency in isotopically pure samples separates faster at low pressures as a result of van der Waals interactions. Because of the extremely low a-axis compressibility, the intralayer …

Materials scienceSublinear functionPhonon02 engineering and technology01 natural sciencessymbols.namesakeRaman scattering experimentsCondensed Matter::Superconductivity0103 physical sciencesPhonomsGraphite010306 general physicsScalingCondensed matter physicsPhysical Systems021001 nanoscience & nanotechnologyTechniquesSemiconductorsRaman spectroscopyCompressibilitysymbolsvan der Waals forceGraphene0210 nano-technologyRaman spectroscopyRaman scattering
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