Bio-metal-organic frameworks for molecular recognition and sorbent extraction of hydrophilic vitamins followed by their determination using HPLC-UV
A bio-metal-organic framework (bio-MOF) derived from the amino acid L-serine has been prepared in bulk form and evaluated as sorbent for the molecular recognition and extraction of B-vitamins. The functional pores of bio-MOF exhibit high amounts of hydroxyl groups jointly directing other supramolecular host-guest interactions thus providing the recognition of B-vitamins in fruit juices and energy drinks. Single-crystal X-ray diffraction studies reveal the specific B-vitamin binding sites and the existence of multiple hydrogen bonds between these target molecules and the framework. It offered unique snapshots to accomplish an efficient capture of these solutes in complex aqueous matrices. Fo…
Efficient Gas Separation and Transport Mechanism in Rare Hemilabile Metal–Organic Framework
Understanding/visualizing the established interactions between gases and adsorbents is mandatory to implement better performance materials in adsorption/separation processes. Here we report the unique behavior of a rare example of a hemilabile chiral three-dimensional metal–organic framework (MOF) with an unprecedented qtz-e-type topology, with formula CuII2(S,S)-hismox·5H2O (1) (hismox = bis[(S)-histidine]oxalyl diamide). 1 exhibits a continuous and reversible breathing behavior, based on the hemilability of carboxylate groups from l-histidine. In situ powder (PXRD) and single crystal X-ray diffraction (SCXRD) using synchrotron radiation allowed us to unveil the crystal structures of four …
Soluble/MOF-Supported Palladium Single Atoms Catalyze the Ligand-, Additive-, and Solvent-Free Aerobic Oxidation of Benzyl Alcohols to Benzoic Acids.
Metal single-atom catalysts (SACs) promise great rewards in terms of metal atom efficiency. However, the requirement of particular conditions and supports for their synthesis, together with the need of solvents and additives for catalytic implementation, often precludes their use under industrially viable conditions. Here, we show that palladium single atoms are spontaneously formed after dissolving tiny amounts of palladium salts in neat benzyl alcohols, to catalyze their direct aerobic oxidation to benzoic acids without ligands, additives, or solvents. With this result in hand, the gram-scale preparation and stabilization of Pd SACs within the functional channels of a novel methyl-cystein…
Selective and Efficient Removal of Mercury from Aqueous Media with the Highly Flexible Arms of a BioMOF
A robust and water-stable metal-organic framework (MOF), featuring hexagonal channels decorated with methionine residues (1), selectively captures toxic species such as CH3 Hg(+) and Hg(2+) from water. 1 exhibits the largest Hg(2+) uptake capacity ever reported for a MOF, decreasing the [Hg(2+) ] and [CH3 Hg(+) ] concentrations in potable water from highly hazardous 10 ppm to the much safer values of 6 and 27 ppb, respectively. Just like with biological systems, the high-performance metal capture also involves a molecular recognition process. Both CH3 Hg(+) and Hg(2+) are efficiently immobilized by specific conformations adopted by the flexible thioether "claws" decorating the pores of 1. T…
Multivariate Metal-Organic Frameworks for the Simultaneous Capture of Organic and Inorganic Contaminants from Water
We report a new water-stable multivariate (MTV) Metal-Organic Framework (MOF) prepared by combining two different oxamide-based metalloligands derived from the natural amino acids L-serine and L-methionine. This unique material features hexagonal channels decorated with two types of flexible and functional 'arms' (-CH2OH and -CH2CH2SCH3) capable to act, synergistically, for the simultaneous and efficient removal of both inorganic (heavy metals like Hg2+, Pb2+ and Tl+) and organic (dyes such as Pyronin Y, Auramine O, Brilliant Green and Methylene Blue) contaminants and, in addition, this MTV-MOF is completely reusable. Single-crystal X-ray diffraction (SCXRD) measurements allowed to solve th…
Highly Efficient MOF-Driven Silver Subnanometer Clusters for the Catalytic Buchner Ring Expansion Reaction
The preparation of novel efficient catalysts-that could be applicable in industrially important chemical processes-has attracted great interest. Small subnanometer metal clusters can exhibit outstanding catalytic capabilities, and thus, research efforts have been devoted, recently, to synthesize novel catalysts bearing such active sites. Here, we report the gram-scale preparation of Ag2subnanometer clusters within the channels of a highly crystalline three-dimensional anionic metal-organic framework, with the formula [Ag2]@AgNa{Ni[Cu(Mempba)]}·48HO [Mempba= N,N′-2,4,6-trimethyl-1,3-phenylenebis(oxamate)]. The resulting crystalline solid catalyst-fully characterized with the help of single-c…
Stabilized Ru[(H2O)(6)](3+) in Confined Spaces (MOFs and Zeolites) Catalyzes the lmination of Primary Alcohols under Atmospheric Conditions with Wide Scope
[EN] Imines are ubiquitous intermediates in organic synthesis, and the metal-mediated imination of alcohols is one of the most direct and simple methods for their synthesis. However, reported protocols lack compatibility with many other functional groups since basic supports/media, pure oxygen atmospheres, and/or released hydrogen gas are required during reaction. Here we show that, in contrast to previous metal-catalyzed methods, hexa-aqueous Ru(III) catalyzes the imination of primary alcohols with very wide functional group tolerance, at slightly acid pH and under low oxygen atmospheres. The inorganic metal complex can be supported and stabilized, integrally, within either faujasite-type …
Self-assembly of catalytically-active supramolecular coordination compounds within metal-organic frameworks
[EN] Supramolecular coordination compounds (SCCs) represent the power of coordination chemistry methodologies to self-assemble discrete architectures with targeted properties. SCCs are generally synthesized in solution, with isolated fully coordinated metal atoms as structural nodes, thus severely limited as metal-based catalysts. Metal-organic frameworks (MOFs) show unique features to act as chemical nanoreactors for the in situ synthesis and stabilization of otherwise not accessible functional species. Here, we present the self-assembly of Pd-II SCCs within the confined space of a pre-formed MOF (SCCs@MOF) and its post-assembly metalation to give a Pd-II-Au-III supra molecular assembly, c…
The MOF-driven synthesis of supported palladium clusters with catalytic activity for carbene-mediated chemistry
The development of catalysts able to assist industrially important chemical processes is a topic of high importance. In view of the catalytic capabilities of small metal clusters, research efforts are being focused on the synthesis of novel catalysts bearing such active sites. Here we report a heterogeneous catalyst consisting of Pd4 clusters with mixed-valence 0/+1 oxidation states, stabilized and homogeneously organized within the walls of a metal-organic framework (MOF). The resulting solid catalyst outperforms state-of-the-art metal catalysts in carbene-mediated reactions of diazoacetates, with high yields (>90%) and turnover numbers (up to 100,000). In addition, the MOF-supported Pd4 c…
Efficient Capture of Organic Dyes and Crystallographic Snapshots by a Highly Crystalline Amino-Acid-Derived Metal-Organic Framework
The presence of residual organic dyes in water resources or wastewater treatment systems, derived mainly from effluents of different industries, is a major environmental problem with no easy solution. Herein, an ecofriendly, water-stable metal-organic framework was prepared from a derivative of the natural amino acid l-serine. Its functional channels are densely decorated with highly flexible l-serine residues bearing hydroxyl groups. The presence of such a flexible and functional environment within the confined environment of the MOF leads to efficient removal of different organic dyes from water: Pyronin Y, Auramine O, Methylene Blue and Brilliant Green, as unveiled by unprecedented snaps…
Cover Picture: Solid-State Molecular Nanomagnet Inclusion into a Magnetic Metal-Organic Framework: Interplay of the Magnetic Properties (Chem. Eur. J. 2/2016)
A post-synthetic approach triggers selective and reversible sulphur dioxide adsorption on a metal-organic framework.
We report the application of a post-synthetic solid-state cation-exchange process to afford a novel 3D MOF with hydrated barium cations hosted at pores able to trigger selective and reversible SO2 adsorption. Computational modelling supports the full reversibility of the adsorption process on the basis of weak supramolecular interactions between SO2 and coordinated water molecules.
Solvent-Dependent Self-Assembly of an Oxalato-Based Three-Dimensional Magnet Exhibiting a Novel Architecture.
The old but evergreen family of bimetallic oxalates still offers innovative and interesting results. When (Me4N)3[Cr(ox)3]·3H2O is reacted with Mn(II) ions in a nonaqueous solvent, a novel three-dimensional magnet of the formula [N(CH3)4]6[Mn3Cr4(ox)12]·6CH3OH is obtained instead of the one-dimensional compound obtained in water. This new material exhibits an unprecedented stoichiometry with a binodal (3,4) net topology and the highest critical temperature (TC = 7 K) observed so far in a manganese-chromium oxalate based magnet.
Metal–organic framework technologies for water remediation: towards a sustainable ecosystem
Having access to clean water is a mandatory requirement for the proper development of living beings. So, addressing the removal of contaminants from aquatic systems should be a priority research topic in order to restore ecosystem balance and secure a more sustainable future. The fascinating structures and striking physical properties of metal–organic frameworks (MOFs) have revealed them as excellent platforms for the removal of harmful species from water. In this review, we have focused our attention on critically highlighting the latest developments achieved in the adsorptive removal of inorganic – metal cations, inorganic acids, oxyanions/cations, nuclear wastes and other inorganic anion…
Bioinspired Metal-Organic Frameworks in Mixed Matrix Membranes for Efficient Static/Dynamic Removal of Mercury from Water
The mercury removal efficiency of a novel metal-organic framework (MOF) derived from the amino acid S-methyl-L-cysteine is presented and the process is characterized by single-crystal X-ray crystallography. A feasibility study is further presented on the performance of this MOF and also that of another MOF derived from the amino acid L-methionine when used as the sorbent in mixed matrix membranes (MMMs). These MOF-based MMMs exhibit high efficiency and selectivity in both static and dynamic regimes in the removal of Hg2+ from aqueous environments, due to the high density of thioalkyl groups decorating MOF channels. Both MMMs are capable to reduce different concentration of the pollutant to …
A Biocompatible Aspartic-Decorated Metal–Organic Framework with Tubular Motif Degradable under Physiological Conditions
Achieving a precise control of the final structure of metal–organic frameworks (MOFs) is necessary to obtain desired physical properties. Here, we describe how the use of a metalloligand design strategy and a judicious choice of ligands inspired from nature is a versatile approach to succeed in this challenging task. We report a new porous chiral MOF, with the formula Ca5II{CuII10[(S,S)-aspartamox]5}·160H2O (1), constructed from Cu2+ and Ca2+ ions and aspartic acid-decorated ligands, where biometal Cu2+ ions are bridged by the carboxylate groups of aspartic acid moieties. The structure of MOF 1 reveals an infinite network of basket-like cages, built by 10 crystallographically distinct Cu(II…
Postsynthetic Approach for the Rational Design of Chiral Ferroelectric Metal–Organic Frameworks
International audience; Ferroelectrics (FEs) are materials of paramount importance with a wide diversity of applications. Herein, we propose a postsynthetic methodology for the smart implementation of ferroelectricity in chiral metal−organic frameworks (MOFs): following a single-crystal to single-crystal cation metathesis, the Ca2+ counterions of a preformed chiral MOF of formula Ca6II{CuII24[(S,S)-hismox]12(OH2)3}·212H2O (1), where hismox is a chiral ligand derived from the natural amino acid l-histidine, are replaced by CH3NH3+. The resulting compound, (CH3NH3)12{CuII24[(S,S)-hismox]12(OH2)3}·178H2O (2), retains the polar space group of 1 and is ferroelectric below 260 K. These results op…
Front Cover: Efficient Capture of Organic Dyes and Crystallographic Snapshots by a Highly Crystalline Amino-Acid-Derived Metal-Organic Framework (Chem. Eur. J. 67/2018)
A novel oxalate-based three-dimensional coordination polymer showing magnetic ordering and high proton conductivity
A novel three-dimensional (3D) coordination polymer with the formula (C3N2H5)4[MnCr2(ox)6]·5H2O (2), where ox = oxalate and C3N2H5 = imidazolium cation, is reported. Single crystal X-ray diffraction reveals that this porous coordination polymer adopts a chiral three-dimensional quartz-like architecture, with the guest imidazolium cations and water molecules being hosted in its pores. This novel multifunctional material exhibits both a ferromagnetic ordering at TC = 3.0 K, related to the host MnCr2 network, and high proton conductivity [1.86 × 10−3 S cm−1 at 295 K and 88% relative humidity (RH)] due to the presence of the acidic imidazolium cations and free water molecules. The similarity of…
Fine-tuning of the confined space in microporous metal–organic frameworks for efficient mercury removal
Offsetting the impact of human activities on the biogeochemical cycle of mercury has become necessary for a sustainable planet. Herein, we report the development of a water-stable and eco-friendly metal–organic framework, which has the formula {Cu4II[(S,S)-methox]2}·5H2O (1), where methox is bis[(S)-methionine]oxalyl diamide. Its features include narrow functional channels decorated with thioalkyl chains, which are able to capture HgCl2 from aqueous media in an efficient, selective, and rapid manner. The conscious design effort in terms of size, shape, and reactivity of the channels results in extremely efficient immobilization of HgCl2 guest species in a very stable conformation, similar t…
Solid-State Molecular Nanomagnet Inclusion into a Magnetic Metal-Organic Framework: Interplay of the Magnetic Properties.
Single-ion magnets (SIMs) are the smallest possible magnetic devices and are a controllable, bottom-up approach to nanoscale magnetism with potential applications in quantum computing and high-density information storage. In this work, we take advantage of the promising, but yet insufficiently explored, solid-state chemistry of metal-organic frameworks (MOFs) to report the single-crystal to single-crystal inclusion of such molecular nanomagnets within the pores of a magnetic MOF. The resulting host-guest supramolecular aggregate is used as a playground in the first in-depth study on the interplay between the internal magnetic field created by the long-range magnetic ordering of the structur…
Synthesis of Densely Packaged, Ultrasmall Pt02Clusters within a Thioether-Functionalized MOF: Catalytic Activity in Industrial Reactions at Low Temperature
The gram-scale synthesis, stabilization, and characterization of well-defined ultrasmall subnanometric catalytic clusters on solids is a challenge. The chemical synthesis and X-ray snapshots of Pt02 clusters, homogenously distributed and densely packaged within the channels of a metal-organic framework, is presented. This hybrid material catalyzes efficiently, and even more importantly from an economic and environmental viewpoint, at low temperature (25 to 140 °C), energetically costly industrial reactions in the gas phase such as HCN production, CO2 methanation, and alkene hydrogenations. These results open the way for the design of precisely defined catalytically active ultrasmall metal c…
Double Interpenetration in a Chiral Three-Dimensional Magnet with a (10,3)-a Structure
A unique chiral three-dimensional magnet with an overall racemic double-interpenetrated (10,3)-a structure of the formula [(S)-(1-PhEt)Me3N]4[Mn4Cu6(Et2pma)12](DMSO)3]·3DMSO·5H2O (1; Et2pma = N-2,6-diethylphenyloxamate) has been synthesized by the self-assembly of a mononuclear copper(II) complex acting as a metalloligand toward Mn(II) ions in the presence of a chiral cationic auxiliary, constituting the first oxamato-based chiral coordination polymer exhibiting long-range magnetic ordering.
Tuning the selectivity of light hydrocarbons in natural gas in a family of isoreticular MOFs
Purification of methane from other light hydrocarbons in natural gas is a topic of intense research due to its fundamental importance in the utilization of natural gas fields. Porous materials have emerged as excellent alternative platforms to conventional cryogenic methodologies to perform this task in a cost- and energy-efficient manner. Here we report a new family of isoreticular chiral MOFs, prepared from oxamidato ligands derived from natural amino acids L-alanine, L-valine and L-leucine, where, by increasing the length of the alkyl residue of the amino acid, the charge density of the MOF's channels can be tuned (1 > 2 > 3), decreasing the adsorption preference towards methane over lig…
Selective Gold Recovery and Catalysis in a Highly Flexible Methionine-Decorated Metal–Organic Framework
A novel chiral 3D bioMOF exhibiting functional channels with thio-alkyl chains derived from the natural amino acid l-methionine (1) has been rationally prepared. The well-known strong affinity of gold for sulfur derivatives, together with the extremely high flexibility of the thioether "arms" decorating the channels, account for a selective capture of gold(III) and gold(I) salts in the presence of other metal cations typically found in electronic wastes. The X-ray single-crystal structures of the different gold adsorbates Au(III)@1 and Au(I)@1 suggest that the selective metal capture occurs in a metal ion recognition process somehow mimicking what happens in biological systems and protein r…
Confined Pt-1(1+) Water Clusters in a MOF Catalyze the Low-Temperature Water-Gas Shift Reaction with both CO2 Oxygen Atoms Coming from Water
[EN] The synthesis and reactivity of single metal atoms in a low-valence state bound to just water, rather than to organic ligands or surfaces, is a major experimental challenge. Herein, we show a gram-scale wet synthesis of Pt-1(1+) stabilized in a confined space by a crystallographically well-defined first water sphere, and with a second coordination sphere linked to a metal-organic framework (MOF) through electrostatic and H-bonding interactions. The role of the water cluster is not only isolating and stabilizing the Pt atoms, but also regulating the charge of the metal and the adsorption of reactants. This is shown for the low-temperature water-gas shift reaction (WGSR: CO + H2O CO2 + H…
Metal–Organic Frameworks as Playgrounds for Reticulate Single-Molecule Magnets
Achieving an accurate control on the final structure of Metal-Organic Frameworks (MOFs) is mandatory to obtain target physical properties. Here we describe how the combination of a metalloligand design strategy and a post-synthetic method is a versatile and powerful approach to success on this extremely difficult task. In a first stage, a novel oxamato-based tetranuclear cobalt(III) complex with a tetrahedron-shape geometry is used, for the first time, as metalloligand toward cal-cium(II) cations to lead a diamagnetic Ca(II)-Co(III) three-dimensional (3D) MOF (1). In a second stage, in a single-crystal to single-crystal manner the calcium(II) ions are replaced by terbium (III), dysprosium(I…
Lanthanide Discrimination with Hydroxyl-Decorated Flexible Metal–Organic Frameworks
We report two new highly crystalline metal-organic frameworks (MOFs), derived from the natural amino acids serine (1) and threonine (2), featuring hexagonal channels densely decorated with hydroxyl groups belonging to the amino acid residues. Both 1 and 2 are capable of discriminating, via solid-phase extraction, a mixture of selected chloride salts of lanthanides on the basis of their size, chemical affinity, and/or the flexibility of the network. In addition, this discrimination follows a completely different trend for 1 and 2 because of the different locations of the hydroxyl groups in each compound, which is evocative of steric complementarity between the substrate and receptor. Last bu…
Crystallographic snapshots of host–guest interactions in drugs@metal–organic frameworks: towards mimicking molecular recognition processes
We report a novel metal–organic framework (MOF) featuring functional pores decorated with hydroxyl groups derived from the natural amino acid L-serine, which is able to establish specific interactions of different natures, strengths and directionalities with organic molecules of technological interest, i.e. ascorbic acid, pyridoxine, bupropion and 17-β-estradiol, based on their different sizes and chemical natures. The ability of 1 to distinctly organize guest molecules within its channels, through the concomitant effect of different directing supramolecular host–guest interactions, enables gaining unique insights, by means of single-crystal X-ray crystallography, into the host–guest intera…
MOF-Triggered Synthesis of Subnanometer Ag02 Clusters and Fe3+ Single Atoms: Heterogenization Led to Efficient and Synergetic One-Pot Catalytic Reactions
Isolated Fe(III)-O Sites Catalyze the Hydrogenation of Acetylene in Ethylene Flows under Front-End Industrial Conditions
[EN] The search for simple, earth-abundant, cheap, and nontoxic metal catalysts able to perform industrial hydrogenations is a topic of interest, transversal to many catalytic processes. Here, we show that isolated FeIII¿O sites on solids are able to dissociate and chemoselectively transfer H2 to acetylene in an industrial process. For that, a novel, robust, and highly crystalline metal¿organic framework (MOF), embedding FeIII¿OH2 single sites within its pores, was prepared in multigram scale and used as an efficient catalyst for the hydrogenation of 1% acetylene in ethylene streams under front-end conditions. Cutting-edge X-ray crystallography allowed the resolution of the crystal structur…
Structural Studies on a New Family of Chiral BioMOFs
The use of a family of dinuclear copper(II) complexes, prepared from enantiopure disubstituted oxamidato ligands derived from the natural amino acids l-alanine, l-valine, and l-leucine, as metalloligands toward barium(II) cations leads to the formation of three novel three-dimensional (3D) chiral metal–organic frameworks (MOFs). They exhibit different architectures, which serve as playground to study both how the chiral information contained in the starting enantiopure ligands is ultimately transmitted to the 3D structure and the effect of the size of the aliphatic residue of the amino acid on the final architecture.
Metal-Organic Frameworks as Chemical Nanoreactors: Synthesis and Stabilization of Catalytically Active Metal Species in Confined Spaces
ConspectusSince the advent of the first metal-organic frameworks (MOFs), we have witnessed an explosion of captivating architectures with exciting physicochemical properties and applications in a wide range of fields. This, in part, can be understood under the light of their rich host-guest chemistry and the possibility to use single-crystal X-ray diffraction (SC-XRD) as a basic characterization tool. Moreover, chemistry on preformed MOFs, applying recent developments in template-directed synthesis and postsynthetic methodologies (PSMs), has shown to be a powerful synthetic tool to (i) tailor MOFs channels of known topology via single-crystal to single-crystal (SC-SC) processes, (ii) impart…
Hydrolase–like catalysis and structural resolution of natural products by a metal–organic framework
[EN] The exact chemical structure of non-crystallising natural products is still one of the main challenges in Natural Sciences. Despite tremendous advances in total synthesis, the absolute structural determination of a myriad of natural products with very sensitive chemical functionalities remains undone. Here, we show that a metal-organic framework (MOF) with alcohol-containing arms and adsorbed water, enables selective hydrolysis of glycosyl bonds, supramolecular order with the so-formed chiral fragments and absolute determination of the organic structure by single-crystal X-ray crystallography in a single operation. This combined strategy based on a biomimetic, cheap, robust and multigr…
CCDC 1891588: Experimental Crystal Structure Determination
Related Article: Marta Mon, Rosaria Bruno, Estefanía Tiburcio, Aida Grau-Atienza, Antonio Sepúlveda-Escribano, Enrique V. Ramos-Fernandez, Alessio Fuoco, Elisa Esposito, Marcello Monteleone, Johannes C. Jansen, Joan Cano, Jesús Ferrando-Soria, Donatella Armentano, Emilio Pardo|2019|Chem.Mater.|31|5856|doi:10.1021/acs.chemmater.9b01995
CCDC 1995182: Experimental Crystal Structure Determination
Related Article: Estefanía Tiburcio, Rossella Greco, Marta Mon, Jordi Ballesteros-Soberanas, Jesús Ferrando-Soria, Miguel López-Haro, Juan Carlos Hernández-Garrido, Judit Oliver-Meseguer, Carlo Marini, Mercedes Boronat, Donatella Armentano, Antonio Leyva-Pérez, Emilio Pardo|2021|J.Am.Chem.Soc.|143|2581|doi:10.1021/jacs.0c12367
CCDC 1823995: Experimental Crystal Structure Determination
Related Article: Marta Mon, Rosaria Bruno, Jesús Ferrando-Soria, Lucia Bartella, Leonardo Di Donna, Marianna Talia, Rosamaria Lappano, Marcello Maggiolini, Donatella Armentano, Emilio Pardo|2018|Materials Horizons|5|683|doi:10.1039/C8MH00302E
CCDC 1558089: Experimental Crystal Structure Determination
Related Article: Marta Mon, Xiaoni Qu, Jesús Ferrando-Soria, Isaac Pellicer-Carreño, Antonio Sepúlveda-Escribano, Enrique V. Ramos-Fernandez, Johannes C. Jansen, Donatella Armentano, Emilio Pardo|2017|J.Mater.Chem.A|5|20120|doi:10.1039/C7TA06199D
CCDC 1530550: Experimental Crystal Structure Determination
Related Article: Thais Grancha, Marta Mon, Jesús Ferrando-Soria, Jorge Gascon, Beatriz Seoane, Enrique V. Ramos-Fernandez, Donatella Armentano, Emilio Pardo|2017|J.Mater.Chem.A|5|11032|doi:10.1039/C7TA01179B
CCDC 1558090: Experimental Crystal Structure Determination
Related Article: Marta Mon, Xiaoni Qu, Jesús Ferrando-Soria, Isaac Pellicer-Carreño, Antonio Sepúlveda-Escribano, Enrique V. Ramos-Fernandez, Johannes C. Jansen, Donatella Armentano, Emilio Pardo|2017|J.Mater.Chem.A|5|20120|doi:10.1039/C7TA06199D
CCDC 1587822: Experimental Crystal Structure Determination
Related Article: Marta Mon, Miguel A. Rivero-Crespo, Jesffls Ferrando-Soria, Alejandro Vidal-Moya, Mercedes Boronat, Antonio Leyva-Pérez, Avelino Corma, Juan C. Hernandez-Garrido, Miguel Lopez-Haro, José J. Calvino, Giulio Ragazzon, Alberto Credi, Donatella Armentano, Emilio Pardo|2018|Angew.Chem.,Int.Ed.|57|6186|doi:10.1002/anie.201801957
CCDC 1938637: Experimental Crystal Structure Determination
Related Article: Lucas H. G. Kalinke, Danielle Cangussu, Marta Mon, Rosaria Bruno, Estefania Tiburcio, Francesc Lloret, Donatella Armentano, Emilio Pardo, Jesus Ferrando-Soria|2019|Inorg.Chem.|58|14498|doi:10.1021/acs.inorgchem.9b02086
CCDC 1938635: Experimental Crystal Structure Determination
Related Article: Lucas H. G. Kalinke, Danielle Cangussu, Marta Mon, Rosaria Bruno, Estefania Tiburcio, Francesc Lloret, Donatella Armentano, Emilio Pardo, Jesus Ferrando-Soria|2019|Inorg.Chem.|58|14498|doi:10.1021/acs.inorgchem.9b02086
CCDC 2007971: Experimental Crystal Structure Determination
Related Article: Rosaria Bruno, Marta Mon, Paula Escamilla, Jesus Ferrando‐Soria, Elisa Esposito, Alessio Fuoco, Marcello Monteleone, Johannes C. Jansen, Rosangela Elliani, Antonio Tagarelli, Donatella Armentano, Emilio Pardo|2021|Adv.Funct.Mater.|31|2008499|doi:10.1002/adfm.202008499
CCDC 1826456: Experimental Crystal Structure Determination
Related Article: Marta Mon, Rosaria Bruno, Rosangela Elliani, Antonio Tagarelli, Xiaoni Qu, Sanping Chen, Jesús Ferrando-Soria, Donatella Armentano, Emilio Pardo|2018|Inorg.Chem.|57|13895|doi:10.1021/acs.inorgchem.8b02409
CCDC 1416018: Experimental Crystal Structure Determination
Related Article: Thais Grancha, Marta Mon, Francesc Lloret, Jesús Ferrando-Soria, Yves Journaux, Jorge Pasán, and Emilio Pardo|2015|Inorg.Chem.|54|8890|doi:10.1021/acs.inorgchem.5b01738
CCDC 1826450: Experimental Crystal Structure Determination
Related Article: Marta Mon, Rosaria Bruno, Rosangela Elliani, Antonio Tagarelli, Xiaoni Qu, Sanping Chen, Jesús Ferrando-Soria, Donatella Armentano, Emilio Pardo|2018|Inorg.Chem.|57|13895|doi:10.1021/acs.inorgchem.8b02409
CCDC 1826452: Experimental Crystal Structure Determination
Related Article: Marta Mon, Rosaria Bruno, Rosangela Elliani, Antonio Tagarelli, Xiaoni Qu, Sanping Chen, Jesús Ferrando-Soria, Donatella Armentano, Emilio Pardo|2018|Inorg.Chem.|57|13895|doi:10.1021/acs.inorgchem.8b02409
CSD 1409698: Experimental Crystal Structure Determination
Related Article: Marta Mon, Miguel A. Rivero-Crespo, Jesffls Ferrando-Soria, Alejandro Vidal-Moya, Mercedes Boronat, Antonio Leyva-Pérez, Avelino Corma, Juan C. Hernandez-Garrido, Miguel Lopez-Haro, José J. Calvino, Giulio Ragazzon, Alberto Credi, Donatella Armentano, Emilio Pardo|2018|Angew.Chem.,Int.Ed.|57|6186|doi:10.1002/anie.201801957
CCDC 1486650: Experimental Crystal Structure Determination
Related Article: Marta Mon, Francesc Lloret, Jesús Ferrando-Soria, Carlos Martí-Gastaldo, Donatella Armentano, Emilio Pardo|2016|Angew.Chem.,Int.Ed.|55|1167|doi:10.1002/anie.201606015
CCDC 1892911: Experimental Crystal Structure Determination
Related Article: Rosa Adam, Marta Mon, Rossella Greco, Lucas H. G. Kalinke, Alejandro Vidal-Moya, Antonio Fernandez, Richard E. P. Winpenny, Antonio Dom��nech-Carb��, Antonio Leyva-P��rez, Donatella Armentano, Emilio Pardo, Jes��s Ferrando-Soria|2019|J.Am.Chem.Soc.|141|10350|doi:10.1021/jacs.9b03914
CCDC 1555659: Experimental Crystal Structure Determination
Related Article: Marta Mon, Julia Vallejo, Jorge Pasán, Oscar Fabelo, Cyrille Train, Michel Verdaguer, Shin-ichi Ohkoshi, Hiroko Tokoro, Kosuke Nakagawa, Emilio Pardo|2017|Dalton Trans.|46|15130|doi:10.1039/C7DT03415F
CCDC 1843114: Experimental Crystal Structure Determination
Related Article: Marta Mon, Rosaria Bruno, Estefanía Tiburcio, Pierre‐Edouard Casteran, Jesús Ferrando‐Soria, Donatella Armentano, Emilio Pardo|2018|Chem.-Eur.J.|24|17712|doi:10.1002/chem.201803547
CCDC 1938638: Experimental Crystal Structure Determination
Related Article: Lucas H. G. Kalinke, Danielle Cangussu, Marta Mon, Rosaria Bruno, Estefania Tiburcio, Francesc Lloret, Donatella Armentano, Emilio Pardo, Jesus Ferrando-Soria|2019|Inorg.Chem.|58|14498|doi:10.1021/acs.inorgchem.9b02086
CCDC 1530549: Experimental Crystal Structure Determination
Related Article: Thais Grancha, Marta Mon, Jesús Ferrando-Soria, Jorge Gascon, Beatriz Seoane, Enrique V. Ramos-Fernandez, Donatella Armentano, Emilio Pardo|2017|J.Mater.Chem.A|5|11032|doi:10.1039/C7TA01179B
CCDC 1891577: Experimental Crystal Structure Determination
Related Article: Marta Mon, Rosaria Bruno, Estefanía Tiburcio, Aida Grau-Atienza, Antonio Sepúlveda-Escribano, Enrique V. Ramos-Fernandez, Alessio Fuoco, Elisa Esposito, Marcello Monteleone, Johannes C. Jansen, Joan Cano, Jesús Ferrando-Soria, Donatella Armentano, Emilio Pardo|2019|Chem.Mater.|31|5856|doi:10.1021/acs.chemmater.9b01995
CCDC 1478222: Experimental Crystal Structure Determination
Related Article: Marta Mon, Jesús Ferrando-Soria, Thais Grancha, Francisco R. Fortea-Pérez, Jorge Gascon, Antonio Leyva-Pérez, Donatella Armentano, and Emilio Pardo|2016|J.Am.Chem.Soc.|138|7864|doi:10.1021/jacs.6b04635
CCDC 1843112: Experimental Crystal Structure Determination
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CCDC 1826453: Experimental Crystal Structure Determination
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CCDC 1541852: Experimental Crystal Structure Determination
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CCDC 2155456: Experimental Crystal Structure Determination
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CCDC 1486651: Experimental Crystal Structure Determination
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CCDC 1891583: Experimental Crystal Structure Determination
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CCDC 2155455: Experimental Crystal Structure Determination
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CCDC 1558088: Experimental Crystal Structure Determination
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CCDC 1826458: Experimental Crystal Structure Determination
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CCDC 1823991: Experimental Crystal Structure Determination
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CCDC 1826454: Experimental Crystal Structure Determination
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CCDC 1826455: Experimental Crystal Structure Determination
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CCDC 1891594: Experimental Crystal Structure Determination
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CCDC 1823993: Experimental Crystal Structure Determination
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CCDC 1493129: Experimental Crystal Structure Determination
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CCDC 1892914: Experimental Crystal Structure Determination
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CCDC 1891591: Experimental Crystal Structure Determination
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CCDC 1478221: Experimental Crystal Structure Determination
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CCDC 1891582: Experimental Crystal Structure Determination
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CCDC 1486649: Experimental Crystal Structure Determination
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CCDC 1891587: Experimental Crystal Structure Determination
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CCDC 1891590: Experimental Crystal Structure Determination
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CCDC 1985884: Experimental Crystal Structure Determination
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CCDC 1891593: Experimental Crystal Structure Determination
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CCDC 1823992: Experimental Crystal Structure Determination
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CCDC 1891579: Experimental Crystal Structure Determination
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CCDC 1891584: Experimental Crystal Structure Determination
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CCDC 1846740: Experimental Crystal Structure Determination
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CCDC 1891576: Experimental Crystal Structure Determination
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CCDC 1995184: Experimental Crystal Structure Determination
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CCDC 1841425: Experimental Crystal Structure Determination
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CCDC 1891580: Experimental Crystal Structure Determination
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CCDC 1478223: Experimental Crystal Structure Determination
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CCDC 1414395: Experimental Crystal Structure Determination
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CCDC 1826457: Experimental Crystal Structure Determination
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CCDC 1891586: Experimental Crystal Structure Determination
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CCDC 1826449: Experimental Crystal Structure Determination
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CCDC 2075709: Experimental Crystal Structure Determination
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CCDC 1995183: Experimental Crystal Structure Determination
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CCDC 1493131: Experimental Crystal Structure Determination
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CCDC 1835021: Experimental Crystal Structure Determination
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CCDC 1891581: Experimental Crystal Structure Determination
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CCDC 1493130: Experimental Crystal Structure Determination
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CCDC 1841391: Experimental Crystal Structure Determination
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CCDC 1921930: Experimental Crystal Structure Determination
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CCDC 1517224: Experimental Crystal Structure Determination
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CCDC 2157534: Experimental Crystal Structure Determination
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CCDC 1891592: Experimental Crystal Structure Determination
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CCDC 1843113: Experimental Crystal Structure Determination
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CCDC 1541853: Experimental Crystal Structure Determination
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CCDC 1555658: Experimental Crystal Structure Determination
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CCDC 2007972: Experimental Crystal Structure Determination
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CCDC 1826451: Experimental Crystal Structure Determination
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CCDC 1891585: Experimental Crystal Structure Determination
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CCDC 1843115: Experimental Crystal Structure Determination
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CCDC 1480930: Experimental Crystal Structure Determination
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CCDC 1587821: Experimental Crystal Structure Determination
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CCDC 1823994: Experimental Crystal Structure Determination
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CCDC 1841392: Experimental Crystal Structure Determination
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CCDC 1921928: Experimental Crystal Structure Determination
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CCDC 1891578: Experimental Crystal Structure Determination
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CCDC 1985885: Experimental Crystal Structure Determination
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CCDC 1891589: Experimental Crystal Structure Determination
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CCDC 1892912: Experimental Crystal Structure Determination
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CCDC 1891595: Experimental Crystal Structure Determination
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CCDC 1891596: Experimental Crystal Structure Determination
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CCDC 1921929: Experimental Crystal Structure Determination
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CCDC 1938636: Experimental Crystal Structure Determination
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CCDC 1517225: Experimental Crystal Structure Determination
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