0000000001299211

AUTHOR

Klaus Jurkschat

showing 54 related works from this author

Cyclic Dinuclear Organotin Cations Stabilized by Bulky Substituents

2015

The syntheses of sterically congested 2,2-bis(diorganochloridostannyl)propane, Me2C(SnClR2)2 (1; R = CH(SiMe3)2), the related salts [cyclo-{Me2C(SnR2)2X}B(ArF)4] (2, X = Cl; 3, X = OAc; 4, X = OH; ArF = 3,5-(CF3)2C6H3), and the four-membered-ring cyclo-{Me2C(SnR2)2O} (5) are reported. The compounds have been characterized by elemental and EDX analyses, 1H, 11B, 13C, 19F, 29Si, and 119Sn NMR and IR spectroscopy, electrospray ionization mass spectrometry, and single-crystal X-ray diffraction analysis.

Inorganic ChemistrySteric effectschemistry.chemical_compoundChemistryPropaneElectrospray ionizationOrganic ChemistryOrganic chemistryInfrared spectroscopyPhysical and Theoretical ChemistryMedicinal chemistryOrganometallics
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The First Examples of a Crown Ether Intramolecularly Encapsulating Mono- and Diorganotin Dications: Synthesis and Structures of [PhSnCH2([16]crown-5)…

2010

The reaction of silver perchlorate with [PhI 2 SnCH 2 ([16]crown-5)] (1) and [I 3 SnCH 2 ([16]crown-5)] (2) gave the organotin(IV)-substituted crown ether complexes [PhSnCH 2 ([16]crown-5)][ClO 4 ] 2 (3) and [HOSnCH 2 ([16]crown-5)][Y] 2 (4: Y= ClO 4 , 5: Y=CF3 S 03 ) , respectively. All compounds have been isolated as air-stable materials and characterised by 1 H, 13 C, 119 Sn and 119 Sn MAS (5) NMR spectroscopy, ESIMS spectrometry, elemental analysis and by single-crystal X-ray diffraction analysis. The molecular structures of 3-5 show that the tin(IV) cation fits perfectly into the crown ether cavity and is coordinated by the five oxygen atoms of the ring to give a pentagonal bipyramidal…

chemistry.chemical_classificationStereochemistryOrganic ChemistryGeneral ChemistryNuclear magnetic resonance spectroscopyRing (chemistry)Silver perchlorateCatalysisCrown CompoundsDicationchemistry.chemical_compoundCrystallographyPentagonal bipyramidal molecular geometrychemistryX-ray crystallographyCrown etherChemistry - A European Journal
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Syntheses, Structures and Reactivity of New Intramolecularly Coordinated Tin Alkoxides Based on an Enantiopure Ephedrine Derivative

2011

The syntheses of the tin compounds [LSn]2 (2), spiro-L2Sn (3), [LSnW(CO)5]2 (4), [LSnBr2]2 (5), spiro-L2Sn·SnBr4 (6) and LSn[OC(O)Ph]2 (8), where L = MeN(CH2CMe2O)[(S)-CH(Me)-(R)-CH(Ph)O], and (Ph4P)2SnBr6 (7) are reported. The compounds were characterized by elemental analysis, multinuclear NMR spectroscopy including 119Sn cross polarisation–magic angle spinning NMR (CP–MAS) (2, 3–6), electrospray ionization mass spectrometry (2–4) and single crystal X-ray diffraction analysis (2, 2·C7H8, 3a, 3b, 4·C7H8, 5, 6·C7H8, 7).

ChemistryStereochemistryElectrospray ionizationchemistry.chemical_elementNuclear magnetic resonance spectroscopyMedicinal chemistryInorganic Chemistrychemistry.chemical_compoundEnantiopure drugElemental analysisReactivity (chemistry)TinSingle crystalDerivative (chemistry)European Journal of Inorganic Chemistry
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Darstellung und struktur von (EtO)2P(O)CH2Si(Me)2CH2SnMe2Cl—ein sechsringchelat mit sesselkonformation und PO ⋯ Sn(Cl)Me2CH2-trigonaler bipyramide a…

1992

Abstract The title compound (EtO)2P(O)CH2Si(Me)2CH2SnMe2Cl (2) has been synthesized by reaction of the new functional Grignard reagent (EtO)2P(O)CH2CH2SiMe2CH2MgCl with Me3SnCl and subsequent treatment with Me2SnCl2. 2 crystallizes in the non-centrosymmetric orthorhombic space group P212121. The structure was refined to a final R-value of 0.0476. The tin atom is pentacoordinated and exhibits a nearly ideal trigonal-bipyramidal coordination (SnCl 2.518(3), Sn ⋯ O 2.371(5) A). This coordination results from a 6-membered chelate involving a chair conformation. The structure of 2 is compared with analogous compounds containing a PO ⋯ Sn- or CO ⋯ Sn-coordination in the first place and a noncy…

MetalationStereochemistryOrganic ChemistryCyclohexane conformationchemistry.chemical_elementCrystal structureRing (chemistry)BiochemistryMedicinal chemistryInorganic ChemistrychemistryX-ray crystallographyMaterials ChemistryMoleculeOrthorhombic crystal systemPhysical and Theoretical ChemistryTinJournal of Organometallic Chemistry
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Dimeres und Trimers 1-Methyl-1-aza-5-stannabicyclo[3.3.01,5]-octan sulfid [MeN(CH2CH2CH2)2SnS]n, Röntgenstrukturanalyse des Dimeren und Gleichgewicht…

1991

Abstract The crystal structure of the dimeric title compound has been determined and refined to R = 0.0266. The core of the nearly centrosymmetric dimer is formed by an almost perfect [SnS]2 rectangle (Sn-S 2.39 and 2.51 A). The two sulfur atoms of this rectangle establish the connecting edge of two distorted trigonal bipyramids around the two tin atoms (Sn … N 2.55 A). Solutions of the title compound contain in addition to the dimer (σ(119Sn) = −4.6 ppm) about 20% of the trimer (+ 10.3 ppm). By quick crystallization a mixture of both oligomers can be transferred into the solid state.

Bicyclic moleculeChemistryDimerOrganic ChemistryTrimerCrystal structureBiochemistrylaw.inventionInorganic ChemistryBond lengthCrystallographychemistry.chemical_compoundMolecular geometrylawX-ray crystallographyMaterials ChemistryPhysical and Theoretical ChemistryCrystallizationJournal of Organometallic Chemistry
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The Influence of Intramolecular Coordination and Ring Strain on the Polymerization Potential of Cyclic Stannasiloxanes

2008

PolymerizationChemistryIntramolecular forcePhotochemistryX ray analysisRing-opening polymerizationRing strain
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Organotin(IV) derivatives containing heteroditopic pyridyl-quinolin-8-olate ligands: Synthesis and structures

2021

Abstract Six novel neutral organotin(IV) complexes, viz. [n-Bu2Sn(L4-PyAQ)2] 1, [Bz2Sn(L4-PyAQ)2] 2, [Ph2Sn(L4-PyAQ)2] 3, [Ph2Sn(L3-PyAQ)2] 4, [Bz3Sn(L4-PyAQ)] 5 and [Ph3Sn(L4-PyAQ)] 6 have been synthesized via reactions of 3/4-pyridyl-quinolin-8-ol pro-ligands, with appropriate diorganotin oxide and triorganotin hydroxide precursors, respectively. The compounds 1-6 were characterized in solution by means of NMR spectroscopy while the solid-state structures of 1, 6, and of the solvates 2·1.5C6H6, 3·0.25C6H6, 2·4·C6H6, and 5·0.5H2O were authenticated by single crystal X-ray diffraction analysis. In the solid-state, the tin centers in 1-2·4·C6H6 are hexacoordinated and reveal a distorted cis-…

010405 organic chemistryChemistryOrganic ChemistryOxidechemistry.chemical_elementNuclear magnetic resonance spectroscopy010402 general chemistry01 natural sciencesBiochemistrySquare pyramidal molecular geometry0104 chemical sciencesInorganic ChemistryCrystallographychemistry.chemical_compoundMaterials ChemistryHydroxidePhysical and Theoretical ChemistryTinSingle crystalJournal of Organometallic Chemistry
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Ring size control in diorganotin sulphides by intramolecular SnN coordination

1992

Abstract The synthesis of intramolecularly coordinated organotin sulphides, [(Me2N CH2CH2CH2)2SnS]n (1) and [Me2NCH2CH2CH2Sn(Ph)S]n (2), is described. Compounds 1 and 2 are dimers in chloroform solution (n = 2). Compound 1 forms a centrosymmetric dimer with a planar rectangular Sn2S2 four-membered ring in its centre. The tin atoms show a distorted trans-cis-cis octahedral coordination by 2C, 2N and 2S. The tin-nitrogen distances are 2.810(3) and 3.158(5) A. Compound 1 can be regarded as a model substance for nucleophilic attack at penta-coordinate tin centres. Although the degree of intramolecular coordination of nitrogen to tin is temperature dependent, the four-membered Sn2Sn2 ring remain…

Intramolecular reactionTertiary amineStereochemistryDimerchemistry.chemical_elementCrystal structureRing (chemistry)Inorganic ChemistryRing sizeCrystallographychemistry.chemical_compoundchemistryIntramolecular forceMaterials ChemistryPhysical and Theoretical ChemistryTinPolyhedron
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Diorganotin Compounds Containing α‐Aminoacidato Schiff Base Ligands Derived from Functionalized 2‐Hydroxy‐5‐(aryldiazenyl)benzaldehyde. Syntheses, St…

2020

Inorganic ChemistryBenzaldehydechemistry.chemical_compoundSchiff basechemistryHydrogen sulfidePolymer chemistrychemistry.chemical_elementTinEuropean Journal of Inorganic Chemistry
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On the Reaction of (tBu2SnO)3 with Organochlorosilanes. Simple Formation of [(tBu2SnO)2(tBu2SiO)]

2008

ChemistrySimple (abstract algebra)Analytical chemistryPhysical chemistryX ray analysis
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On the reaction of [Ph2(OH)Si]2O with t-Bu2SnCl2: Synthesis and characterization of the first well defined polystannasiloxane [(t-Bu2SnO)(Ph2SiO)2]n

1997

Abstract The high yield synthesis of [(t-Bu2SnO)(Ph2SiO)2], 1 is reported. Compound 1 is a linear polymer in the solid state but a six-membered ring in solution.

chemistry.chemical_classificationSiliconOrganic Chemistrychemistry.chemical_elementPolymerCharacterization (mathematics)Ring (chemistry)BiochemistryInorganic ChemistryCrystallographychemistryYield (chemistry)X-ray crystallographyMaterials ChemistryPhysical and Theoretical ChemistryWell-definedTinJournal of Organometallic Chemistry
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Nucleophilic attack within Ge, Sn and Pb complexes containing Me2N(CH2)(3) - as a potential intramolecular donor ligand

1998

Abstract Thirteen tin compounds LxPhySnClz and LPh2SnPhX (x=1–4, y=0–3, z=0–2, XPh, F, Cl, Br, I, OPh), six germanium compounds LxPhyGeClz and four lead compounds LPh2PbPhX (XPh, Cl, Br, I) containing the potential intramolecular donor LMe2N(CH2)3—have been synthesized by Grignard reactions, redistribution, halogenation, exchange of halide and phenylation. Evidence for 1,5-chelation in which the donor Me2N intramolecularly attacks the Lewis-acidic atoms Ge, Sn or Pb is provided by six crystal structure determinations: Me2N(CH2)3SnPh2Cl, 5; Me2N(CH2)3SnPh2Br, 5a; Me2N(CH2)3SnPh2I, 5b; Me2N(CH2)3SnPh2OPh, 5d; Me2N(CH2)3SnPh3·HCl·H2O. 1a; Me2N(CH2)3PbPh2I, 17b), and by solution 13C, 119Sn a…

StereochemistryChemistryLigandChemical shiftHalogenationNuclear magnetic resonance spectroscopyCrystal structureInorganic ChemistryElectronegativityCrystallographyNucleophileIntramolecular forceMaterials ChemistryPhysical and Theoretical Chemistry
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Intramolecularly Coordinated Bis(crown ether)-Substituted Organotin Halides as Ditopic Salt Receptors

2013

The synthesis of the bis(crown ether)-substituted organostannanes X2Sn(CH2-[16]-crown-5)2 (3, X = I; 4, X = Br; 5, X = Cl; 6, X = F) and X2Sn(CH2-[13]-crown-4)2 (10, X = I; 11, X = Br; 12, X = F) is reported. The compounds have been characterized by 1H, 13C, 19F, and 119Sn NMR spectroscopy, elemental analyses, and electrospray ionization mass spectrometry (ESI-MS). Single-crystal X-ray diffraction analyses reveal a distorted-octahedral cis,cis,trans configuration of the tin atoms in compounds 4–6 and 10–12 as a result of intramolecular O→Sn coordination. The ability of the host molecules to form mono- and ditopic complexes with various halide salts in different solvents, including water, ha…

chemistry.chemical_classificationStereochemistryElectrospray ionizationOrganic Chemistrychemistry.chemical_elementHalideSalt (chemistry)Nuclear magnetic resonance spectroscopyMedicinal chemistryInorganic ChemistrychemistryIntramolecular forceMoleculePhysical and Theoretical ChemistryTinCrown etherOrganometallics
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Trapping Molecular SnBr 2 (OH) 2 by Tin Alkoxide Coordination: Syntheses and Molecular Structures of [MeN(CH 2 CMe 2 O) 2 SnBr 2 ] 2 ·SnBr 2 (OH) 2 a…

2012

The synthesis of the intramolecularly coordinated stannylenes and their transition-metal complexes of the type RN(CH2CMe2O)2SnL [1: L = lone pair, R = Me; 2: L = lone pair, R = n-octyl; 5: L =W(CO)5, R = Me; 6: L = Cr(CO)5, R = Me; 7: L =W(CO)5, R = n-octyl; 8: L = Fe(CO)4, R = Me], and of the tin(IV) compounds RN(CH2CMe2O)2SnBr2 (9: R = Me), [MeN(CH2CMe2O)2SnBr2]2·SnBr2(OH)2 (10) and spiro-[RN(CH2CMe2O)2]2Sn (3: R = Me; 4: R = n-octyl) is reported. The compounds were characterized by elemental analyses, 1H, 13C, 119Sn, and 119Sn magic-angle spinning (5, 6) NMR spectroscopy, electrospray mass spectrometry, and single-crystal X-ray diffraction analysis.

Inorganic chemistrychemistry.chemical_elementTrappingNuclear magnetic resonance spectroscopyMedicinal chemistryInorganic Chemistrychemistry.chemical_compoundTransition metalchemistryAlkoxideX-ray crystallographyAlkanolamineTinLone pairEuropean Journal of Inorganic Chemistry
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Cis versus Trans: The Coordination Environment about the Tin(IV) Atom in Spirocyclic Amino Alcohol Derivatives.

2018

The syntheses of amino alcohols MeN(CH2 CH2 CMe2 OH)2 (1), MeN(CMe2 CH2 OH)(CH2 CMe2 OH) (2), MeN(CH2 CH2 CH2 OH)(CH2 CMe2 OH) (3), MeN(CH2 CH2 CMe2 OH)(CH2 CMe2 OH) (4), MeN(CH2 CH2 CMe2 OH)(CH2 CH2 OH) (5), and MeN(CH2 CH2 OH) (CH2 CH2 CH2 OH) (6) as well as spirocyclic tin(IV) alkoxides spiro-[nBuN(CH2 CMe2 O)2 ]2 Sn (7), spiro-[MeN(CH2 CH2 CMe2 O)2 ]2 Sn (8), spiro-[para-FC6 H4 N (CH2 CMe2 O)2 ]2 Sn (9), spiro-[MeN(CMe2 CH2 O)(CH2 CMe2 O)]2 Sn (10), spiro-[MeN(CH2 CH2 CH2 O)(CH2 CMe2 O)]2 Sn (11), spiro-[MeN(CH2 CH2 CMe2 O)(CH2 CMe2 O)]2 Sn (12), spiro-[MeN(CH2 CH2 CMe2 O)(CH2 CH2 O)]2 Sn (13) and spiro-[MeN(CH2 CH2 O)(CH2 CH2 CH2 O)]2 Sn (14) are reported. The compounds were characteri…

010405 organic chemistryOrganic Chemistrychemistry.chemical_elementInfrared spectroscopyAlcoholGeneral Chemistry010402 general chemistry01 natural sciencesMedicinal chemistryCatalysis0104 chemical scienceschemistry.chemical_compoundchemistryAtomTinChemistry (Weinheim an der Bergstrasse, Germany)
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18F-labeling of peptides by means of an organosilicon-based fluoride acceptor.

2006

Fluorine-18 is among the most commonly used radionuclides for positron emission tomography (PET). This non-invasive imaging technique is capable of providing in vivo information about the distribution of radiolabeled biomolecules by 1808 coincidence detection of two simultaneously emitted photons from positron–electron annihilation. Although a number of different radiotracers have been successfully employed in PET, only a few, such as 2-[F]fluoro-2-deoxy-d-glucose (FDG) and [F]fluorodopa, have gained widespread application in nuclear medicine. The reason for this is that the regioselective introduction of F into tracer molecules is often non-specific and radiochemical yields (RCY) of the Fl…

Fluorine RadioisotopesAqueous solutionMolecular StructureInorganic chemistrySynthonRadiochemistryRegioselectivityGeneral ChemistryPeptides CyclicCatalysisPeptide FragmentsIsotopic labelingchemistry.chemical_compoundFluorideschemistryModels ChemicalYield (chemistry)Isotope LabelingMoleculeIndicators and ReagentsOrganosilicon CompoundsAcetonitrileOrganosiliconAngewandte Chemie (International ed. in English)
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Synthesis and structural studies of 2-stannyl-substituted ferrocenylmethylamine and -phosphine derivatives 2-Me2RSnFcCH2Y (RMe, Cl; YNMe2, PPh2, P(…

1995

Abstract 2-(Trimethylstannyl)ferrocenylmethyldiphenylphosphine, 2-Me3SnFcCH2PPh2 (2a), was synthesized from 2-Me3SnFcCH2NMe2 (1a) and Ph2PH. Compound 2a is oxidized with H2O2 to 2-Me3SnFcCH2P(O)Ph2 (3a). Halogenation of 1a and 2a with Me2SnCl2 and 3a with HCl-diethyl ether yields the organotin monochlorides 2-Me3(Cl)SnFcCH2Y ( 1b , Y = NMe 2 ; 2b , Y = PPh 2 3b , Y = P ( O ) Ph 2 ) . Both crystal structure determinations and multinuclear magnetic resonance studies in solution reveal for 1b–3b molecular structures in which the tin atom approaches a trigonal bipyramidal pentacoordination as a consequence of an intramolecular Y Sn interaction. The donor strength of Y increases in the order PPh2

StereochemistryOrganic ChemistryHalogenationchemistry.chemical_elementEtherCrystal structureBiochemistryMedicinal chemistryInorganic Chemistrychemistry.chemical_compoundTrigonal bipyramidal molecular geometryFerrocenechemistryIntramolecular forceMaterials ChemistryPhysical and Theoretical ChemistryTinPhosphineJournal of Organometallic Chemistry
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18F-Markierung von Peptiden mithilfe eines Organosilicium-Fluoridacceptors

2006

StereochemistryChemistryGeneral MedicineAngewandte Chemie
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Novel Stannatrane N(CH2CMe2O)2(CMe2CH2O)SnO-t-Bu and Related Oligonuclear Tin(IV) Oxoclusters. Two Isomers in One Crystal

2016

The syntheses of the alkanolamine N(CH2CMe2OH)2(CMe2CH2OH) (1), of the stannatrane N(CH2CMe2O)2(CMe2CH2O)SnO-t-Bu (2), and of the trinuclear tin oxocluster 3 consisting of the two isomers [(μ3-O)(O-t-Bu){Sn(OCH2CMe2)(OCMe2CH2)2N}3] (3a) and [(μ3-O)(μ3-O-t-Bu){Sn(OCH2CMe2)(OCMe2CH2)2N}3] (3b) as well as the isolation of a few crystals of the hexanuclear tin oxocluster [LSnOSn(OH)3LSnOH]2 [L = N(CH2CMe2O)2(CMe2CH2O)] (4) are reported. The compounds were characterized by 1H, 13C, 15N, and 119Sn (1–3) nuclear magnetic resonance and infrared spectroscopy, electrospray ionization mass spectrometry, and single-crystal X-ray diffraction analysis (1–4). A graph set analysis was performed for compoun…

010405 organic chemistryChemistryElectrospray ionizationAnalytical chemistryInfrared spectroscopychemistry.chemical_element010402 general chemistry01 natural sciencesGraph0104 chemical sciencesInorganic ChemistryCrystalCrystallographychemistry.chemical_compoundDensity functional theoryAlkanolaminePhysical and Theoretical ChemistryTinInorganic Chemistry
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CCDC 1409484: Experimental Crystal Structure Determination

2015

Related Article: Michael Wagner, Bernhard Zobel, Christina Dietz, Dieter Schollmeyer, and Klaus Jurkschat|2015|Organometallics|34|5602|doi:10.1021/acs.organomet.5b00829

Space GroupCrystallographyCrystal SystemCrystal Structure(mu-propane-22-diyl)-tetrakis(bis(trimethylsilyl)methyl)-dichloro-di-tin acetone solvateCell ParametersExperimental 3D Coordinates
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CCDC 1409486: Experimental Crystal Structure Determination

2015

Related Article: Michael Wagner, Bernhard Zobel, Christina Dietz, Dieter Schollmeyer, and Klaus Jurkschat|2015|Organometallics|34|5602|doi:10.1021/acs.organomet.5b00829

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(mu-acetato)-(mu-propane-22-diyl)-tetrakis(bis(trimethylsilyl)methyl)-di-tin tetrakis(35-bis(trifluoromethyl)phenyl)borateExperimental 3D Coordinates
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CCDC 2066256: Experimental Crystal Structure Determination

2021

Related Article: Tushar S. Basu Baul, Anurag Chaurasiya, Banteilang Lyngdoh Nonglait, Antonin Lyčka, Dieter Schollmeyer, Klaus Jurkschat|2021|J.Organomet.Chem.|946-947|121898|doi:10.1016/j.jorganchem.2021.121898

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinatesdi-n-butyl-bis(5-((pyridin-4-yl)diazenyl)quinolin-8-olato)-tin(iv) unknown solvate
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CCDC 2066261: Experimental Crystal Structure Determination

2021

Related Article: Tushar S. Basu Baul, Anurag Chaurasiya, Banteilang Lyngdoh Nonglait, Antonin Lyčka, Dieter Schollmeyer, Klaus Jurkschat|2021|J.Organomet.Chem.|946-947|121898|doi:10.1016/j.jorganchem.2021.121898

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterstriphenyl-(5-((pyridin-4-yl)diazenyl)quinolin-8-olato)-tin(iv)Experimental 3D Coordinates
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CCDC 1483889: Experimental Crystal Structure Determination

2016

Related Article: Britta Glowacki, Michael Lutter, Dieter Schollmeyer, Wolf Hiller, and Klaus Jurkschat|2016|Inorg.Chem.|55|10218|doi:10.1021/acs.inorgchem.6b01429

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters1-t-Butoxido-(289-trioxa-5-aza-33771111-tetramethyl-1-stannatricyclo[3.3.3.015]undecane)Experimental 3D Coordinates
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CCDC 1858288: Experimental Crystal Structure Determination

2018

Related Article: Britta Glowacki, Roman Pallach, Michael Lutter, Fabian Roesler, Hazem Alnasr, Dieter Schollmeyer, Cederic Thomas, Klaus Jurkschat|2018|Chem.-Eur.J.|24|19266|doi:10.1002/chem.201803952

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters2-((2-hydroxy-2-methylpropyl)(methyl)amino)-2-methylpropan-1-olExperimental 3D Coordinates
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CCDC 1936179: Experimental Crystal Structure Determination

2020

Related Article: Tushar Shubhra Basu Baul, Anurag Chaurasiya, Monosh Rabha, Snehadrinarayan Khatua, Antonin Lyčka, Dieter Schollmeyer, Klaus Jurkschat|2020|Eur.J.Inorg.Chem.|2020|1803|doi:10.1002/ejic.202000177

Space GroupCrystallographyCrystal SystemCrystal Structuredibutyl-[N-({2-oxido-5-[(4-nitrophenyl)diazenyl]phenyl}methylidene)phenylalaninato]-tin(iv)Cell ParametersExperimental 3D Coordinates
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CCDC 1858294: Experimental Crystal Structure Determination

2018

Related Article: Britta Glowacki, Roman Pallach, Michael Lutter, Fabian Roesler, Hazem Alnasr, Dieter Schollmeyer, Cederic Thomas, Klaus Jurkschat|2018|Chem.-Eur.J.|24|19266|doi:10.1002/chem.201803952

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parametersbis(2-((2-oxido-2-methylpropyl)(methyl)amino)-2-methylpropan-1-olato)-tinExperimental 3D Coordinates
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CCDC 1936182: Experimental Crystal Structure Determination

2020

Related Article: Tushar Shubhra Basu Baul, Anurag Chaurasiya, Monosh Rabha, Snehadrinarayan Khatua, Antonin Lyčka, Dieter Schollmeyer, Klaus Jurkschat|2020|Eur.J.Inorg.Chem.|2020|1803|doi:10.1002/ejic.202000177

catena-[(mu-N-{[2-oxido-5-(phenyldiazenyl)phenyl]methylidene}leucinato)-dienzyl-tin]Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 902177: Experimental Crystal Structure Determination

2013

Related Article: Verena Arens, Christina Dietz, Dieter Schollmeyer, and Klaus Jurkschat|2013|Organometallics|32|2775|doi:10.1021/om400216z

Space GroupCrystallographyCrystal SystemCrystal Structurebis(Iodo)-bis(14710-tetraoxacylcotridec-12-ylmethyl)-tin(iv)Cell ParametersExperimental 3D Coordinates
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CCDC 902179: Experimental Crystal Structure Determination

2013

Related Article: Verena Arens, Christina Dietz, Dieter Schollmeyer, and Klaus Jurkschat|2013|Organometallics|32|2775|doi:10.1021/om400216z

Space GroupCrystallographyDifluoro-bis(14710-tetraoxacylcotridec-12-ylmethyl)-tin(iv)Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 902174: Experimental Crystal Structure Determination

2013

Related Article: Verena Arens, Christina Dietz, Dieter Schollmeyer, and Klaus Jurkschat|2013|Organometallics|32|2775|doi:10.1021/om400216z

Dibromo-bis((1471013-pentaoxacyclohexadec-15-yl)methyl)-tin(iv)Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1936180: Experimental Crystal Structure Determination

2020

Related Article: Tushar Shubhra Basu Baul, Anurag Chaurasiya, Monosh Rabha, Snehadrinarayan Khatua, Antonin Lyčka, Dieter Schollmeyer, Klaus Jurkschat|2020|Eur.J.Inorg.Chem.|2020|1803|doi:10.1002/ejic.202000177

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(mu-N-({2-oxido-5-[(4-nitrophenyl)diazenyl]phenyl}methylidene)tryptophanato)-(N-({2-oxido-5-[(4-nitrophenyl)diazenyl]phenyl}methylidene)tryptophanato)-tetra-n-butyl-di-tin (N-({2-oxido-5-[(4-nitrophenyl)diazenyl]phenyl}methylidene)tryptophanato)-di-n-butyl-tinExperimental 3D Coordinates
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CCDC 902178: Experimental Crystal Structure Determination

2013

Related Article: Verena Arens, Christina Dietz, Dieter Schollmeyer, and Klaus Jurkschat|2013|Organometallics|32|2775|doi:10.1021/om400216z

Space GroupCrystallographyDibromo-bis(14710-tetraoxacylcotridec-12-ylmethyl)-tin(iv)Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 902175: Experimental Crystal Structure Determination

2013

Related Article: Verena Arens, Christina Dietz, Dieter Schollmeyer, and Klaus Jurkschat|2013|Organometallics|32|2775|doi:10.1021/om400216z

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersDichloro-bis((1471013-pentaoxacyclohexadec-15-yl)methyl)-tin(iv)Experimental 3D Coordinates
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CCDC 1483890: Experimental Crystal Structure Determination

2016

Related Article: Britta Glowacki, Michael Lutter, Dieter Schollmeyer, Wolf Hiller, and Klaus Jurkschat|2016|Inorg.Chem.|55|10218|doi:10.1021/acs.inorgchem.6b01429

Space GroupCrystallographyCrystal System(mu3-oxido)-(mu3-t-butanolato)-tris(mu2-bis(2-dimethyl-2-oxidopropyl)(1-dimethyl-2-oxidopropyl)amine)-tri-tin (mu3-oxido)-(mu3-bis(2-dimethyl-2-oxidopropyl)(1-dimethyl-2-oxidopropyl)amine)-bis(mu2-bis(2-dimethyl-2-oxidopropyl)(1-dimethyl-2-oxidopropyl)amine)-(t-butanolato)-tri-tin toluene solvateCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1858297: Experimental Crystal Structure Determination

2018

Related Article: Britta Glowacki, Roman Pallach, Michael Lutter, Fabian Roesler, Hazem Alnasr, Dieter Schollmeyer, Cederic Thomas, Klaus Jurkschat|2018|Chem.-Eur.J.|24|19266|doi:10.1002/chem.201803952

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinatesbis(3-((2-oxidoethyl)(methyl)amino)propan-1-olato)-tin
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CCDC 1483888: Experimental Crystal Structure Determination

2016

Related Article: Britta Glowacki, Michael Lutter, Dieter Schollmeyer, Wolf Hiller, and Klaus Jurkschat|2016|Inorg.Chem.|55|10218|doi:10.1021/acs.inorgchem.6b01429

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parametersbis(2-dimethyl-2-hydroxypropyl)(1-dimethyl-2-hydroxypropyl)amineExperimental 3D Coordinates
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CCDC 2066260: Experimental Crystal Structure Determination

2021

Related Article: Tushar S. Basu Baul, Anurag Chaurasiya, Banteilang Lyngdoh Nonglait, Antonin Lyčka, Dieter Schollmeyer, Klaus Jurkschat|2021|J.Organomet.Chem.|946-947|121898|doi:10.1016/j.jorganchem.2021.121898

Space GroupCrystallographytribenzyl-(5-((pyridin-4-yl)diazenyl)quinolin-8-olato)-tin(iv) hemihydrateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1496144: Experimental Crystal Structure Determination

2016

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Space GroupCrystallographybis(mu-2-[bis(2-oxido-2-methylpropyl)amino]-2-methylpropan-1-olato)-tetrakis(mu-hydroxo)-bis(mu-oxido)-bis(2-[bis(2-oxido-2-methylpropyl)amino]-2-methylpropan-1-olato)-tetrahydroxo-hexa-tin benzene solvateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 2066257: Experimental Crystal Structure Determination

2021

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parametersdibenzyl-bis(5-((pyridin-4-yl)diazenyl)quinolin-8-olato)-tin(iv) benzene solvateExperimental 3D Coordinates
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CCDC 1858291: Experimental Crystal Structure Determination

2018

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Space GroupCrystallographybis(44'-(methylazanediyl)bis(2-methylbutan-2-olato))-tinCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1858296: Experimental Crystal Structure Determination

2018

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Space GroupCrystallographyCrystal Systembis(4-((2-oxidoethyl)(methyl)amino)-2-methylbutan-2-olato)-tinCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1936181: Experimental Crystal Structure Determination

2020

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Space GroupCrystallographyCrystal Systemcatena-[(mu-N-{[2-oxido-5-(phenyldiazenyl)phenyl]methylidene}leucinato)-dibenzyl-tin]Crystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 902176: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersDifluoro-bis((1471013-pentaoxacyclohexadec-15-yl)methyl)-tin(iv)Experimental 3D Coordinates
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CCDC 2066259: Experimental Crystal Structure Determination

2021

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parametersdibenzyl-bis(5-((pyridin-3-yl)diazenyl)quinolin-8-olato)-tin(iv) benzene solvateExperimental 3D Coordinates
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CCDC 1858292: Experimental Crystal Structure Determination

2018

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Space GroupCrystallographyCrystal Systembis(11'-((4-fluorophenyl)azanediyl)bis(2-methylpropan-2-olato))-tinCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1409487: Experimental Crystal Structure Determination

2015

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(mu-hydroxo)-(mu-propane-22-diyl)-tetrakis(bis(trimethylsilyl)methyl)-di-tin tetrakis(35-bis(trifluoromethyl)phenyl)borateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1858290: Experimental Crystal Structure Determination

2018

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Space GroupCrystallographyCrystal SystemCrystal Structurebis(11'-(butylazanediyl)bis(2-methylpropan-2-olato))-tinCell ParametersExperimental 3D Coordinates
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CCDC 2066258: Experimental Crystal Structure Determination

2021

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Space GroupCrystallographyCrystal SystemCrystal Structurediphenyl-bis(5-((pyridin-4-yl)diazenyl)quinolin-8-olato)-tin(iv) benzene solvateCell ParametersExperimental 3D Coordinates
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CCDC 1858293: Experimental Crystal Structure Determination

2018

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Space GroupCrystallographyCrystal System(11'-((4-fluorophenyl)azanediyl)bis(2-methylpropan-2-olato))-bis(t-butoxy)-tinCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1858295: Experimental Crystal Structure Determination

2018

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Space GroupCrystallographyCrystal Systembis(4-((2-oxidoethyl)(methyl)amino)-2-methylbutan-2-olato)-tin toluene solvateCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1409488: Experimental Crystal Structure Determination

2015

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Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates(mu-oxo)-(mu-propane-22-diyl)-tetrakis(bis(trimethylsilyl)methyl)-di-tin
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CCDC 1409485: Experimental Crystal Structure Determination

2015

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(mu-chloro)-(mu-propane-22-diyl)-tetrakis(bis(trimethylsilyl)methyl)-di-tin tetrakis(35-bis(trifluoromethyl)phenyl)borateExperimental 3D Coordinates
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CCDC 1858289: Experimental Crystal Structure Determination

2018

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters2-hydroxy-N-(1-hydroxy-2-methylpropan-2-yl)-N2-dimethylpropan-1-aminium formateExperimental 3D Coordinates
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