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RESEARCH PRODUCT

Synthesis, microstructure and dielectric properties of (1−x)PSN−xPLuN

Andris SternbergW. ŚMigaRenata Bujakiewicz-korońskaM. BurzyńskaJan SuchaniczMaija AntonovaMaruta DambekalneAnna KalvaneIrena Jankowska-sumaraBarbara Garbarz-glosDorota Sitko

subject

PermittivityPhase transitionMaterials scienceDielectricTrigonal crystal systemMicrostructureCrystallographyPhase (matter)visual_artvisual_art.visual_art_mediumGeneral Materials ScienceCeramicInstrumentationSolid solution

description

Ceramic lead niobates and their solid solutions PSN–PLuN (pure lutecium niobate) were synthesized by solid state reactions. The sequence of phases formed at PSN–PLuN synthesis has been studied by X-ray analysis. Their symmetry changed from rhombohedral for PSN to pseudo-monoclinic for the 0.75PSN–0.25PLuN compositions. The performed EDS investigations revealed that the samples PSN–PLuN are perfectly sintered. They contain a little glassy phase and their grains are well shaped. The increase of lutecium content in the examined solid solution caused downward shift of the temperature of the phase transition. The decrease of the achieved permittivity values ϵ was observed as well.

https://doi.org/10.1080/01411590802457995