Search results for " Reference"

Analytical capabilities of high performance liquid chromatography – Atmospheric pressure photoionization – Orbitrap mass spectrometry (HPLC-APPI-Orbi…

2015

A new analytical method was established and validated for the analysis of 27 brominated flame retardants (BFRs), including so called "emerging" and "novel" BFRs (EBFRs and NBFRs) in fish samples. High performance liquid chromatography (HPLC) coupled to Orbitrap mass spectrometry (Orbitrap-MS) employing atmospheric pressure photoionization (APPI) interface operated in negative mode was used for the identification/quantitation of contaminants. HPLC-Orbitrap-MS analysis provided a fast separation of selected analytes within 14 min, thus demonstrating a high throughput processing of samples. The developed methodology was tested by intralaboratory validation in terms of recovery, repeatability, …

The planar two-body problem for spheroids and disks

2021

We outline a new method suggested by Conway (2016) for solving the two-body problem for solid bodies of spheroidal or ellipsoidal shape. The method is based on integrating the gravitational potential of one body over the surface of the other body. When the gravitational potential can be analytically expressed (as for spheroids or ellipsoids), the gravitational force and mutual gravitational potential can be formulated as a surface integral instead of a volume integral, and solved numerically. If the two bodies are infinitely thin disks, the surface integral has an analytical solution. The method is exact as the force and mutual potential appear in closed-form expressions, and does not invol…

Assessment of Vitamin E Intake in Relation to Tolerable Upper Intake Levels

2018

Assessment of Dietary Intake of Phosphorus in Relation to Tolerable Upper Intake Levels

2018

Assessment of Copper Intake in Relation to Tolerable Upper Intake Levels

2018

Assessment of Zinc Intake in Relation to Tolerable Upper Intake Levels

2018

Assessment of Dietary Intake of Manganese in Relation to Tolerable Upper Intake Level

2019

The Norwegian Scientific Committee for Food and Environment (Vitenskapskomiteen for mat og miljø, VKM) has, at the request of the Norwegian Food Safety Authority (Mattilsynet; NFSA), evaluated the intake of manganese from the diet and 1, 5 or 10 mg manganese per day in food supplements. The former maximum limit for manganese in food supplements was 5 mg per daily dose. 
 Manganese (Mn) is an essential dietary mineral for mammals, and is a component of metalloenzymes such as superoxide dismutase, arginase and pyruvate carboxylase. Manganese is involved in amino acid-, lipid- and carbohydrate metabolism and in proteoglycan synthesis in bone formation. In 2013, the European Food Safety Au…

Recovering bronze metallurgy from archaeological artefacts for the production of reference materials in conservation science

2007

The production of reference Cu-based alloys is the first step of an original experimental protocol to be used in the field of conservation and restoration of metal artefacts. The production of these synthetic alloys has a double value. They can be used both as suitable substitutes of unique archaeological pieces for testing new materials and methods for conservation, and as guidelines for contemporary metal production. We report on a research activity focused on the recovery of the ancient production techniques from the investigation of archaeological copper-based artefacts. The chemical, physical and metallurgical characterization of several Cu-based artefacts, found in different Italian a…

Ceramic production at Selinunte (Sicily) during the 4th and 3rd century BCE: New archaeometric data through the analysis of kiln wastes

2018

Abstract A set of 37 overfired ceramic samples was collected from the dump of two kilns sited in the productive area FF1 in the acropolis of Selinunte (south western Sicily), being specifically active in the period 409–250 BCE. The ceramic samples were analysed by thin-section petrography and chemical analysis, with the aim to establish a valuable ‘reference group’ representative of the ceramic produced at Selinunte during the Punic phase. The petrographic and chemical analyses allowed to state that the ceramic manufactures from the kilns operating in the FF1 insula are characterized by rather homogeneous textural/compositional features. The daily-use common ware here produced is characteri…

mtDNA analysis of the human remains buried in the sarcophagus of Federico II

2005

Abstract The sarcophagus containing the remains of Federico II, located in the Cathedral of Palermo (Sicily, Italy), was opened on 1998 to perform a multidisciplinary survey [1]. Next to the remains of Federico II and in close contact with them were laying two other skeletons belonging, according to historical records, to Pietro II di Aragona and to an anonymous person (“The Third Individual”), probably a woman. The bones appeared severely deteriorated. Chemical analysis performed on bone samples excluded that the bodies underwent some kind of embalming process. The analysis of mtDNA from bone samples taken from the three skeletons was successful in only one of the two labs involved. The HV…