Search results for "OXIDATION"

showing 10 items of 1913 documents

Photooxidations of Alkenes in Fluorinated Constrained Media:  Fluoro-organically Modified NaY as Improved Reactors for Singlet Oxygen “Ene” Reactions

2007

Creating a stationary fluorinated environment inside the zeolite cavity can increase the reactivity observed for intrazeolite photooxidation of alkenes. Exchanging the zeolite with fluorinated organic cations is a much more effective strategy than simply using a fluorinated solvent for slurry irradiations. Use of cations containing C-F bonds is also more efficient than use of deuterated cations for creation of a singlet oxygen friendly environment where the quenching processes are slowed down. Doping the zeolite with fluoro-organic cation 4 resulted in an increase in the singlet oxygen lifetime to 12 micros.

chemistry.chemical_classificationQuenching (fluorescence)ZEOLITESChemistryAlkeneSinglet oxygenOrganic ChemistryInorganic chemistryINTRAZEOLITE PHOTOOXIDATIONSLIFETIMEOXIDATIONPhotochemistrySolventchemistry.chemical_compoundCHEMISTRYReactivity (chemistry)Singlet stateDEACTIVATIONOLEFINSZeoliteEne reactionThe Journal of Organic Chemistry
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Manganese(III)-mediated oxidative carbon-carbon bond cleavage of the 1,10-phenanthroline-5,6-dione ligand

1999

[EN] A new manganese(III)-1,10-phenanthroline-5,6-dione (phendione) complex possessing a putative Mn-2(mu-O) (mu-O2CMe)(2) core has been found to undergo a Ligand-based oxidative cleavage of the C(5)-C(6) bond in weak acid aqueous MeOH under aerobic conditions at room temperature to yield 2,2'-bipyridyl-3,3'-dicarboxylate with co-reduction to the corresponding Mn-II-phendione species.

chemistry.chemical_classificationQuinone complexesPolynuclear complexesAqueous solutionLigandCarboxylato complexesPhenanthrolinechemistry.chemical_elementCrystal structureManganesePhotochemistryCleavage (embryo)Medicinal chemistryInorganic Chemistrychemistry.chemical_compoundchemistryCarbon–carbon bondYield (chemistry)FISICA APLICADACrystal structuresOxidationMaterials ChemistryPhysical and Theoretical ChemistryManganese complexes
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O-Ribosyl-phosphate purine as a constant modified nucleotide located at position 64 in cytoplasmic initiator tRNAsMetof yeasts

1991

The unknown modified nucleotide G*, isolated from both Schizosaccharomyces pombe and Torulopsis utilis initiator tRNAs(Met), has been identified as an O-ribosyl-(1"----2')-guanosine-5"-phosphate, called Gr(p), by means of HPLC, UV-absorption, mass spectrometry and periodate oxidation procedures. By comparison with the previously published structure of Ar(p) isolated from Saccharomyces cerevisiae initiator tRNA(Met), the (1"----2')-glycosidic bond in Gr(p) has been postulated to have a beta-spatial conformation. The modified nucleotide Gr(p) is located at position 64 in the tRNA(Met) molecules, i.e. at the same position as Ar(p). Since we have also characterized Gr(p) in Candida albicans ini…

chemistry.chemical_classificationRNA Transfer MetbiologyPeriodic AcidSaccharomyces cerevisiaeGuanosine MonophosphateGuanosineRNA Fungalbiology.organism_classificationSaccharomycesMass Spectrometrychemistry.chemical_compoundchemistryBiochemistrySchizosaccharomycesGuanosine monophosphateTransfer RNASchizosaccharomyces pombeGeneticsSpectrophotometry UltravioletNucleotideOxidation-ReductionChromatography High Pressure LiquidSchizosaccharomycesCandidaNucleic Acids Research
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Oxidation of N,N-Benzylalkylamines to Nitrones by Mo(VI) and W(VI) Polyperoxo Complexes

1996

Abstract Oxidation of N,N-benzylalkylamines in chloroform by Mo(VI) and W(VI) polyperoxo complexes (PPC) of general formula Q+3{PO4[MO(O2)2]4}3− (Q+ = onium ion) yield the corresponding nitrones as oxidized products quantitatively. Only in the case of N,N-benzylmethylamine the formation of nitrone is accompanied by 25% of benzaldoxime. Oxidation of N,N-benzyltertbutylamine and N,N-benzylisopropylamine follows second order kinetics. This finding does not disqualify the hypothesis that the reaction might occur by a rate determining nucleophilic attack of the amine onto the peroxide oxygens leading, through a Bartlett-type transition state, to the probable formation of the corresponding hydrox…

chemistry.chemical_classificationReaction mechanismLigandStereochemistryPolyperoxo complexesProcess Chemistry and TechnologyN-benzylalkylaminesNPolyperoxo complexes; NN-benzylalkylamines; OxidationMedicinal chemistryPeroxideCatalysisNitroneReaction coordinateAdductchemistry.chemical_compoundHydroxylaminechemistryNucleophileOxidationPhysical and Theoretical Chemistry
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Overview on oxidation mechanisms of organic compounds by TiO2 in heterogeneous photocatalysis

2012

This review provides the reader with a general overview on heterogeneous photocatalytic oxidation mechanisms in the presence of TiO2, with a special address to conversion of aliphatic and aromatic organic species. The aim was to clarify the steps of the photo-oxidation of the various classes of compounds and to relate them with the properties of the catalysts and the experimental conditions used. Reactions carried out to perform complete degradation and photocatalytic partial oxidations have been deeply discussed. Recent isotopic studies highlighted new reaction pathways concerning partial oxidation of alcohols to aldehyde and oxidation of benzene while EPR investigations confirmed that not…

chemistry.chemical_classificationReaction mechanismRadicalOrganic ChemistryPhotochemistryAldehydeCatalysisCatalysischemistry.chemical_compoundchemistryOrganic reactionPhotocatalysisPartial oxidationSettore CHIM/07 - Fondamenti Chimici Delle TecnologiePhysical and Theoretical ChemistryPhotocatalysis Reaction mechanisms Organic reactions TiO2Benzene
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Electrochemical Oxidation of Carboxylic Acids in Water at Boron-Doped Diamond (BDD) Anodes in the Range of Potential of Oxygen Evolution: Detection M…

2013

The electrochemical oxidation in water solutions of selected carboxylic acids (namely oxalic, formic, acetic, maleic, and succinic) at boron-doped diamond (BDD) anodes was investigated by polarization and chronoamperometric measurements. In the presence of low concentrations of carboxylic acids, current densities changed approximately linearly with the acid concentrations. Furthermore, when the current densities were plotted as a function of the chemical oxygen demand, a similar response was observed for all the investigated acids with the exception of oxalic acid. For high carboxylic acid concentrations, the linear variation is often loosen and different behaviors are observed depending on…

chemistry.chemical_classificationReaction mechanismSupporting electrolyteCarboxylic acidInorganic chemistryOxalic acidElectrochemical oxidation BDD ElecrtocatalysisOxygen evolutionchemistry.chemical_elementSettore ING-IND/27 - Chimica Industriale E TecnologicaElectrochemistryCatalysischemistry.chemical_compoundchemistryElectrochemistryChlorine
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Antioxidant compound supplementation prevents oxidative damage in a Drosophila model of Parkinson's disease

2013

Loss-of-function mutations in the DJ-1 gene are linked to rare autosomal recessive forms of parkinsonism. In Drosophila, two DJ-1 orthologs have been identified, DJ-1α and DJ-1β. Several studies have shown that DJ-1β mutant flies are viable and fertile but exhibit age-dependent locomotor defects, shortened life span, and enhanced sensitivity to toxins that induce oxidative stress response compared to control flies. We also demonstrated that long-term dietary supplementation with antioxidant compounds was effective at increasing life-span values of DJ-1β mutants. These results, together with high levels of oxidative stress markers detected in newly eclosed DJ-1β mutant flies compared to cont…

chemistry.chemical_classificationReactive oxygen speciesAntioxidantVitamin Cmedicine.medical_treatmentParkinson DiseaseBiologymedicine.disease_causeProtein oxidationAscorbic acidBiochemistryAntioxidantsSuperoxide dismutaseDisease Models AnimalOxidative StressDrosophila melanogasterchemistryBiochemistryCatalasePhysiology (medical)medicinebiology.proteinAnimalsReactive Oxygen SpeciesOxidative stressFree Radical Biology and Medicine
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Beeinflussung des Leberzellmetabolismus, der Freisetzung von reaktiven Sauerstoffspezies sowie Apoptoseaktivierung durch hypotherme oxygenierte Leber…

2003

Two different methods of liver preservation were compared : simple cold storage (CS) and hypothermic oxygenated perfusion extracorporal (HOPE). After 10 h of preservation (4°C) with modified UW solution reperfusion was performed by isolated liver perfusion for 90 minutes. Reperfusion injury was estimated by release of cytosolic enzymes, formation of superoxide anions, determination of lipid peroxidation, glycolytic metabolites, bileflow and by PCR analysis. The results showed that after cold storage the formation of reactive oxygen species was significant higher as compared with perfused livers. Correspondingly expressions of mediators (TNFα, NF kappa B, MIP-2, SAPK) and apoptosis (Caspase …

chemistry.chemical_classificationReactive oxygen speciesChemistrySuperoxideCold storagemedicine.diseaseMolecular biologyLipid peroxidationchemistry.chemical_compoundImmunologymedicineViaspanLiver preservationReperfusion injuryPerfusion
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Crosstalk between mitochondria and peroxisomes

2015

Mitochondria and peroxisomes are small ubiquitous organelles. They both play major roles in cell metabolism, especially in terms of fatty acid metabolism, reactive oxygen species (ROS) production, and ROS scavenging, and it is now clear that they metabolically interact with each other. These two organelles share some properties, such as great plasticity and high potency to adapt their form and number according to cell requirements. Their functions are connected, and any alteration in the function of mitochondria may induce changes in peroxisomal physiology. The objective of this paper was to highlight the interconnection and the crosstalk existing between mitochondria and peroxisomes. Speci…

chemistry.chemical_classificationReactive oxygen speciesFatty acid metabolismCellReviewMitochondrionBiologyPeroxisomechemistry.chemical_compoundCrosstalk (biology)medicine.anatomical_structurechemistryBiochemistryOrganellemedicineBeta oxidation
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Oxidative stress and mitochondrial failure in the pathogenesis of glaucoma neurodegeneration

2015

This review focuses on oxidative stress and mitochondrial failure for understanding mechanisms of optic nerve damage in primary open-angle glaucoma. The chapter shows scientific evidence for the role of mitochondrial disbalance and reactive oxygen species in glaucoma neurodegeneration. Mitochondria regulate important cellular functions including reactive oxygen species generation and apoptosis. Mitochondrial alterations result from a wide variety of damaging sources. Reactive oxygen species formed by the mitochondria can act as signaling molecules, inducing lipid peroxidation and/or excitotoxicity with the result of cell lesion and death. Antioxidants may help to counteract oxidative stress…

chemistry.chemical_classificationReactive oxygen speciesNeurodegenerationExcitotoxicityMitochondrionBiologymedicine.diseasemedicine.disease_causeNeuroprotectionCell biologyLipid peroxidationchemistry.chemical_compoundchemistryBiochemistryApoptosismedicineOxidative stress
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