0000000000041096
AUTHOR
Eric H. Silver
Microcalorimeter/EBIT measurements of X-ray spectra of highly charged ions
Spectra of highly charged Ar, Kr, Xe and Fe ions, produced in an Electron Beam Ion Trap (EBIT), have been recorded in a broad X-ray energy band (0.2 keV to 10 keV) with a microcalorimeter detector. The first analysis of the Kr spectra has been completed and most of the spectral lines have been identified as transitions of B- to Al-like Kr. Line intensity ratios of Fe XVII have been measured and compared with theoretical models.
Astrophysics and spectroscopy with microcalorimeters on an electron beam ion trap
The importance of the combination of electron beam ion trap (EBIT) spectroscopy with X-ray microcalorimeters in the field of astrophysics was discussed. X-ray astronomy involves heavily charged ion instruments , especially EBIT, to obtain improved quality atomic data. In this regard, the research program at the National Institute of Standards and Technology, which uses X-ray spectroscopic methods to study plasma and atomic physics, was also discussed.
Spectral broadening by incomplete thermalization of the energy in X-ray microcalorimeters with superconducting absorber and NTD-Ge thermal sensor
Abstract We present a model of the response of a cryogenic microcalorimeter with superconducting absorber and phonon sensitive thermal sensor to the absorption of X-ray photons. The model is based on the main microscopic processes responsible for the thermalization of the deposited energy. We use a system of rate equations to describe the energy downconversion in the superconductor and transport to the thermal sensor. The model is a tool to investigate the thermalization efficiency with respect to the device characteristics (i.e. absorber material, geometry), in order to optimize the performances of these detectors. As a first case study, we report results of simulations for a microcalorime…
Xrase: The X-Ray Spectroscopic Explorer
The X-Ray Spectroscopic Explorer (XRASE) has a unique combination of features that will make it possible to address many of NASA’s scientific goals. These include how galaxy clusters form, the physics and chemistry of the ISM, the heating of stellar coronae, the amount and content of intergalactic baryonic matter, the mass of black holes and the formation of disks and jets in AGN and galactic binaries. XRASE has a thin foil, multilayered telescope with a large collecting area up to 10 keV, especially in the Fe Kα region (1100 cm2). Its microcalorimeter array combines high energy resolution (7 eV at 6 keV) and efficiency with a field-of-view of 26 arcmin2. A deep orbit allows for long, conti…
X-ray and gamma-ray astronomy with NTD germanium-based microcalorimeters
We report on the performance of our NTD-Ge microcalorimeters. To date, the spectral resolution for x-ray and gamma-ray lines from radioactive sources and laboratory plasmas is 4.8 eV in the entire 1 - 6 keV band and 52 eV at 60 keV. Technical details responsible for this performance are presented as well as an innovative electro-thermal approach for enhancing count-rate capability.
Test of x-ray microcalorimeters with bilayer absorbers
Superconducting absorbers for thermal X-ray microcalorimeters should convert into thermalized phonons and transfer to the thermal sensor most of the energy deposited by single photons, on a time scale as short as a few tens of microseconds. Since deposition of X-ray energy in a superconductor produces quasiparticles by breaking up of Cooper pairs, the thermalization efficiency depends on the time scale on which they survive within the absorber volume, trapping part of the absorbed energy. According to the predicted values of their microscopic parameters, in many standard type-I superconducting metals the quasiparticle life time at very low temperatures results too long to allow for recombin…
Light weight, thin plastic foil, X-ray telescopes
We present results from a program to develop an X-ray telescope made from thin plastic shells. Our initial results have been obtained from multi-shell cylindrical lenses that are used in a point-to-point configuration to image the small focal spot of a an X-ray tube on a microchannel plate detector. We describe the steps that led up to the present design and present data from the tests that have been used to identify the properties of the plastic material that make it a suitable X-ray reflector. We discuss two applications of our technology to X-ray missions that are designed to address some of the scientific priorities set forth in NASA's long term plans for high energy astrophysics. One m…
Thin-shell plastic lenses for space and laboratory applications
We have identified an inexpensive, readily available, mechanically stable, extremely smooth, elastic, and mechanically uniform plastic suitable for thin film X-ray optics. Polyethylene terephthalate (PET) is easily deformed without losing its elastic properties or surface smoothness. Most important, PET can be coated with mono- or multilayers that reflect X-rays at grazing incidence. We have used these properties to produce X-ray optics made either as a concentric nest of cylinders or as a spiral. We have produced accurately formed shells in precisely machined vacuum mandresl or used a pin and wheel structure to form a continuously wound spiral. The wide range of medical, industrial and sci…
Laboratory astrophysics survey of key x-ray diagnostic lines using a microcalorimeter on an electron beam ion trap
Cosmic plasma conditions created in an electron beam ion trap (EBIT) make it possible to simulate the dependencies of key diagnostic X-ray lines on density, temperature, and excitation conditions that exist in astrophysical sources. We used a microcalorimeter for such laboratory astrophysics studies because it has a resolving power ≈1000, quantum efficiency approaching 100%, and a bandwidth that spans the X-ray energies from 0.2 keV to 10 keV. Our microcalorimeter, coupled with an X-ray optic to increase the effective solid angle, provides a significant new capability for laboratory astrophysics measurements. Broadband spectra obtained from the National Institute of Standards and Technology…
Spectral broadening by spatial effects in X-ray microcalorimeters with superconducting absorber and NTD-Ge thermal sensor
We discuss how the sensitivity to the position of absorption of the photons can affect the spectral resolution of X-ray microcalorimeters with superconducting Sn absorber and NTD-Ge thermal sensor. Data obtained through the computer simulations are reported for microcalorimeters with different geometries and phonon transmission probabilities at the interface between the absorber and thermistor.
A microcalorimeter spectrometer for the investigation of laboratory plasmas
We describe a cryostat and 2-stage ADR specifically designed for making measurements at the NIST EBIT (Electron Beam Ion Trap) facility. The design is compact and consists of a single helium bath with two vapor-cooled shields. The 2-stage ADR has two separate magnets and two heat switches. The interface between the EBIT and microcalorimeter array will also be described.
CALOS: an experiment to study the solar corona with an array of NTD Ge microcalorimeters
In response to the Italian Space Agency announcement "New Ideas for Space Missions", we have proposed an observatory "CALorimetri per Osservazioni Solari" (CALOS) that will perform spatially resolved (Deltatheta similar to 2) X-ray spectroscopy of the solar corona over the 0.1 - 10 keV band using an array of NTD germanium microcalorimeters. The observatory will also include an X-ray polarimeter of radically new design that will study the hard X-ray solar emission and its polarization and will serve as a flare alarm.
Analysis of broadband x-ray spectra of highly charged krypton from a microcalorimeter detector of an electron-beam ion trap
Spectra of highly charged Kr ions, produced in an electron-beam ion trap (EBIT), have been recorded in a broad x-ray energy band (0.3 keV to 4 keV) with a microcalorimeter detector. Most of the spectral lines have been identified as transitions of B- to Al-like Kr. The transition energies have been determined with 0.2% uncertainty. A semi-empirical EBIT plasma model has been created to calculate a synthetic spectrum of highly charged Kr and to determine a charge state distribution of Kr ions inside the EBIT.
Thin plastic shell x-ray optics: an update
We present new results from a program to develop large area X-ray telescopes that are made from thin plastic shells. We use multi-shell cylindrical lenses in a point-to-point configuration to form full aperture images of the small focal spot in a an X-ray tube on a microchannel plate detector. The image data are analyzed to yield radial profiles and encircled energy curves. The derived parameters can be extrapolated to the case of a telescope that is a conical approximation to Wolter 1 optics. The plastic shells can be coated with suitable mono- or multilayers that allow for a wideband coverage of X-ray energies. Our current program is focused on the development of a large area, hard X-ray …
A single stage adiabatic demagnetization refrigerator for testing x-ray microcalorimeters
A single stage Adiabatic Demagnetization Refrigerator (ADR), has been set-up at the X-ray Astronomy Calibration and Testing (XACT) facility of INAF - Osservatorio Astronomico di Palermo G.S. Vaiana, for the development and testing of cryogenic X-ray detectors for laboratory and astrophysical applications. The ADR allows to cool detectors at temperatures below 40 mK and to maintain them at constant operating temperature for many hours. We describe the design and construction of the ADR and present test results and performances.
EBIT diagnostics using X-ray spectra of highly ionized Ne
We have carried out a detailed analysis of highly ionized neon spectra collected at the NIST EBIT using an NTD germanium X-ray microcalorimeter developed at the Harvard-Smithsonian Center for Astrophysics [Nucl. Instr. and Meth. A 444 (2000) 156]. Our attention was focused especially on the Ne IX He-like triplet to check electron density diagnostics through the intercombination/forbidden line ratio. We have investigated possible effects of the ion dynamics on the plasma emission line intensities, looking at the dependence of the count-rate and the charge state distribution on the electron beam energy and current. The temperature and spatial distribution of the neon ions, and hence the overl…
B-MINE, the balloon-borne microcalorimeter nuclear line explorer
B-MINE is a concept for a balloon mission designed to probe the deepest regions of a supernova explosion by detecting Ti-44 emission at 68 keV with spatial and spectral resolutions that are sufficient to determine the extent and velocity distribution of the Ti-44 emitting region. The payload introduces the concept of focusing optics and microcalorimeter spectroscopy to nuclear line emission astrophysics. B-MINE has a thin, plastic foil telescope multilayered to maximize the reflectivity in a 20 keV band centered at 68 keV and a microcalorimeter array optimized for the same energy band. This combination provides a reduced background, an energy resolution of 50 eV and a 3sigma sensitivity in …
A fully planar approach to the construction of X-Ray microcalorimeters with doped Germanium sensors
We have investigated a fully planar technology for the development of arrays of X-ray microcalorimeters with doped germanium thermal sensor. We describe the proposed approach and show promising results obtained with the deep etching of germanium, the most critical step of the whole process.
The constellation-X focal plane microcalorimeter array: An NTD-germanium solution
The hallmarks of Neutron Transmutation Doped (NTD) germanium cryogenic thermistors include high reliability, reproducibility, and long term stability of bulk carrier transport properties. Using micro-machined NTD Ge thermistors with integral “flying” leads, we can now fabricate two-dimensional arrays that are built up from a series of stacked linear arrays. We believe that this modular approach of building, assembling, and perhaps replacing individual modules of detectors is essential to the successful fabrication and testing of large multi-element spectrometers. Details of construction are presented.
High Energy, High Resolution X-Ray Spectroscopy: Microcalorimeters For Nuclear Line Astrophysics
We introduce focusing optics and microcalorimeter spectroscopy to nuclear line emission astrophysics with a balloon payload concept called, B‐MINE. It is designed to probe the deepest regions of a supernova explosion by detecting 44Ti emission at 68 keV with spatial and spectral resolutions that are sufficient to determine the velocity distribution of the 44Ti emitting region. B‐MINE has a thin plastic foil telescope multilayered to maximize the reflectivity in a 20 keV band centered at 68 keV and a microcalorimeter array optimized for the same energy band. This combination provides a reduced background, an energy resolution of 50 eV and a 3σ sensitivity in 106 s of 6 × 10−8 ph cm−2 s−1 at …
Spectral broadening by quasiparticle pile-up in X-ray microcalorimeters with superconducting absorbers
Long-living quasiparticles can pile-up in a superconducting absorber of an X-ray microcalorimeter when photons are detected at high count rate. These quasiparticles can give a non-negligible contribution to the total heat capacity of the detector thus affecting the pulse height spectrum of detected photons. We investigated this effect with numerical simulations and evaluated the resulting spectral broadening as a function of the photon absorption rate, and the heat capacity of the detector for a NTD germanium microcalorimeter with pure Sn absorber.
Emission-Line Intensity Ratios in F[CLC]e[/CLC] [CSC]xvii[/CSC] Observed with a Microcalorimeter on an Electron Beam Ion Trap
We report new observations of emission line intensity ratios of Fe XVII under controlled experimental conditions, using the National Institute of Standards and Technology electron beam ion trap (EBIT) with a microcalorimeter detector. We compare our observations with collisional-radiative models using atomic data computed in distorted wave and R-matrix approximations, which follow the transfer of the polarization of level populations through radiative cascades. Our results for the intensity ratio of the 2p6 1S0-2p53d 1P1 15.014 A line to the 2p6 1S0-2p53d 3D1 15.265 A line are 2.94 ± 0.18 and 2.50 ± 0.13 at beam energies of 900 and 1250 eV, respectively. These results are not consistent wit…
NTD-GE-based microcalorimeter performance
Our group has been developing x-ray microcalorimeters consisting of neutron transmutation doped (NTD) germanium thermistors attached to superconducting tin absorbers. We discuss the performance of single pixel x-ray detectors, and describe an array technology. In this paper we describe the read-out circuit that allows us to measure fast signals in our detectors as this will be important in understanding the primary cause of resolution broadening. We describe briefly a multiplexing scheme that allows a number of different calorimeters to be read out using a single JFET. We list the possible causes of broadening and give a description of the experiment which best demonstrates the cause of the…
Thermalization efficiency of superconducting absorbers for thermal X-ray microcalorimeters
The persistence of long living quasiparticles created in the energy thermalization process can affect the performances of a thermal X-ray microcalorimeter with superconducting absorber. Numerical simulations indicate that in an ab- sorber made of high-purity Sn, operated at temperatures lower than 100 mK, up to 60% of the deposited energy can remain trapped in the quasiparticle system for a time much longer than the time scale of the thermal sensor response, producing a reduction of the SNR of the detector. Other pure superconductors can present the same problem and therefore a microscopic analysis of the physical properties can be useful to identify suitable absorbing materials and optimiz…
Laboratory astrophysics and microanalysis with NTD-germanium-based X-ray microcalorimeters
With the ability to create cosmic plasma conditions in the laboratory it is possible to investigate the dependencies of key diagnostic X-ray lines on density, temperature, and excitation conditions that exist in astrophysical sources with X-ray optics and a high-resolution X-ray microcalorimeter. The same instrumentation can be coupled to scanning electron microscopes or X-ray fluorescence probes to analyze the elemental and chemical composition of electronic, biological, geological and particulate materials. We describe how our microcalorimeter and X-ray optics provide significantly improved capabilities for laboratory astrophysics and microanalysis.
Modeling the energy thermalization of X-ray photons in a microcalorimeter with superconducting absorber
We present a modeling of the response of a microcalorimeter to the absorption of X-ray photons, based on the main microscopical processes responsible for the energy thermalization. In particular, we have modeled a microcalorimeter with superconducting tin absorber (350 micron x 350 micron x 7 micron) and neutron transmutation doped (NTD) germanium thermistor (75 micron x 50 micron x 150 micron). Such a detector, operated at 60 mK, is expected to achieve a spectral resolution as good as 1 eV FWHM in the soft X-ray energy range, based on the known sources of thermal and electronic noise. Nevertheless, the best spectral resolution measured in laboratory experimental tests is of about 5 eV FWHM…